Sciencemadness Discussion Board

organic chemistry thioester preparation

ramarao - 23-9-2006 at 18:53

I would like to prepare thioester of (2-aminothiozolyl )-2-methoxycarbonyl-methoxyimino-3-oxobutanoic acid with Dibenzothiozole disyulphide,using Triethylphosphite as catalyst/oxygen scavenger.Could any one please help me with operating parameters to get highest yield without any residue of TEP oxide in the product.