LD5050
Hazard to Others
Posts: 182
Registered: 16-1-2017
Member Is Offline
Mood: No Mood
|
|
DCM inplace of Ether for recovering Benzaldehyde adduct?
I prepared a Benzaldehyde adduct with Sodium Bisulfite using this method here: https://erowid.org/archive/rhodium/chemistry/eleusis/bisulfi... To recover the Benzaldehyde it says to use Ether, Toluene, or Benzene.. My
question is would it be OK to use DCM instead? I don't see why it wouldn't but I don't want to go ruining all my Benzaldhyde in case for some reason
It shouldn't be used.
|
|
Magpie
lab constructor
Posts: 5939
Registered: 1-11-2003
Location: USA
Member Is Offline
Mood: Chemistry: the subtle science.
|
|
I used DCM in place of ether in my synthesis of salicylaldehyde here: http://www.sciencemadness.org/talk/viewthread.php?tid=61964#...
See the statement in the Conclusions section.
I try to make this substitution whenever possible. Good luck.
The single most important condition for a successful synthesis is good mixing - Nicodem
|
|
LD5050
Hazard to Others
Posts: 182
Registered: 16-1-2017
Member Is Offline
Mood: No Mood
|
|
Thanks Magpie, nice write up btw I like when people include pics.
|
|