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Author: Subject: Synthesis and some properties of 2-amino 4,6-dinitroresorcinol and 2-diazo 4,6-dinitroresorcinol
nitro-genes
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[*] posted on 18-2-2019 at 14:14
Synthesis and some properties of 2-amino 4,6-dinitroresorcinol and 2-diazo 4,6-dinitroresorcinol


Here a rough first version of the copper/ascorbic mediated reduction of styphnic acid to styphnamic acid and some properties of the corresponding diazo derivative. Ha! Another obscure diazoquinone bites the dust! :D

Thoughts, ideas, criticism welcome :) Input on the most likely mechanism by which the cupric/ascorbic mediated reduction works would be especially appreciated. :)

Attachment: Synthesis and some properties of 2-amino 4,6-dinitroresorcinol and 2-diazo 4,6-dinitroresorcinol (rough version).pdf (2.5MB)
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[Edited on 18-2-2019 by nitro-genes]
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[*] posted on 13-7-2019 at 14:30


very good work



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