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Author: Subject: How to make Carbon Tetrachloride
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[*] posted on 20-7-2019 at 07:09

Recommend any one trying this is to use a UV-C sterilizing lamp as net output at lower wattage of UV-C will be way larger.
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[*] posted on 20-7-2019 at 10:48

TCCA will dissolve in chloroform. under UV light with aid of little sulfuric acid (or any other acid as catalyst ) they will react to form CCl4.
as shown below HCl will recycle.
i haven't don this before if i did try i will use addition funnel to drip the mixture to my UV chamber which as mono calcium phosphate granules as solid catalyst. it made from three neck round bottom flask one of which has mercury gas lamp. covered with aluminium foil.
maybe DCM will work too.

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