holmes1880
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Isosorbitol Dinitrate
Isosorbitol Dinitrate:
white microcrystals
empirical formula: C6H8N2O8
molecular weight: 236.1
oxygen balance: –54.2%
nitrogen content: 11.87%
melting point: 70 °C = 158 °F (decomposition)
lead block test: 311 cm3/10 g
detonation velocity, confined:
5300 m/s at r = 1.08 g/cm3
deflagration point: 173 °C = 343 °F
impact sensitivity: 1.5 kp m = 15 N m
friction sensitivity: over 16 kp = 160 N
pistil load crackling
Isosorbitol dinitrate serves as an effective cardial medicine (in low percentage mixture with milk sugar; it is more effective than
W PETN). The pure substance is a strong explosive.
Great properties, great stability, but cannot find much on synthesis.
Discuss.
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The WiZard is In
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Quote: Originally posted by holmes1880  | Isosorbitol Dinitrate:
white microcrystals
empirical formula: C6H8N2O8
molecular weight: 236.1
oxygen balance: –54.2%
nitrogen content: 11.87%
melting point: 70 °C = 158 °F (decomposition)
lead block test: 311 cm3/10 g
detonation velocity, confined:
5300 m/s at r = 1.08 g/cm3
deflagration point: 173 °C = 343 °F
impact sensitivity: 1.5 kp m = 15 N m
friction sensitivity: over 16 kp = 160 N
pistil load crackling
Isosorbitol dinitrate serves as an effective cardial medicine (in low percentage mixture with milk sugar; it is more effective than
W PETN). The pure substance is a strong explosive.
Great properties, great stability, but cannot find much on synthesis.
Discuss. |
The book you cribbed this from fails to mention that it is an oily liquid.
Synthesis is standard.
Curious dobe I — with all the expls in la book, why chose
this one did you? & byda which edition #1-6?
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The WiZard is In
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So sez PATR 2700 G82,
however.....
The hexa can be made as an oily liquid see Davis or (better) Urbanski.
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hissingnoise
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WiZ, you may be thinking of sorbitol hexanitrate which *is* a syrupy liquid - and isomeric with nitromannite.
But isosorbitol dinitrate has a poor OB, low VoD and the LBT puts it just ahead of sucrose octonitrate!
Great properties - I don't think so?
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holmes1880
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Hissingnoise,
I'm looking at certain properties such as stability and deflagration points. PETN is at 3Nm for impact stability.....compare this to 15Nm of I.D. I
like it. Plus, such a high negative OB gives it a nice room for mixing with AN
@ Wizard
Yes, I think you are confusing it, because it clearly states white microcrystals. Anyways, I need to find an economic way to synthesize it.
[Edited on 13-1-2011 by holmes1880]
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TheOrbit
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for drug "medicine" industrial synthesis one of the common reference is
Pharmaceutical manufacturing encyclopedia
search for it and you will find most of the marketing available drug there
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TheOrbit
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and also it preferable to call it (isosorbide dinitrate).
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The WiZard is In
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| Quote: Originally posted by holmes1880 | Hissingnoise,
I'm looking at certain properties such as stability and deflagration points. PETN is at 3Nm for impact stability.....compare this to 15Nm of I.D. I
like it. Plus, such a high negative OB gives it a nice room for mixing with AN |
Time Magazine 17xi10 named the explosive IMX-101 #43 of
the top 50 inventions of the year.
http://tinyurl.com/4q46l9q
http://en.wikipedia.org/wiki/IMX-101
Run it through DTIC.MIL
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The WiZard is In
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It is listed as such in The Merck Index.
[87-33-2]
It refs. Prepn. from sorbitol: Goldberg, Acta Physiol. Scand.
15 173 (1948). C.A. 42, 5564 (1948)
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TheOrbit
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| Quote: Originally posted by The WiZard is In |
It is listed as such in The Merck Index.
[87-33-2]
It refs. Prepn. from sorbitol: Goldberg, Acta Physiol. Scand.
15 173 (1948). C.A. 42, 5564 (1948) |
i said it is PREFERABLE not a must to be named like this.
and it mentioned under isosorbide dinitrate in Merck Index.
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The WiZard is In
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| Quote: Originally posted by TheOrbit |
i said it is PREFERABLE not a must to be named like this.
and it mentioned under isosorbide dinitrate in Merck Index.
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What! I see not were we disagree.
Using my God like powers of reference .... I see you used
the 11th 1989 ed of the Merck Index. 'bout the only change
in the current 14th ed. 2006 [#5225] is the addition of its CA #.
Trivia - What were the first few ed's of what is now called The
Merck index labeled?
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TheOrbit
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there is no disagree , everyone has the right to defend its opinion. i post this name because its the common name used for this drug so it will ease
search
i hope that i misunderstood this "STRANGE" sentence !!!!
| Quote: |
Trivia - What were the first few ed's of what is now called The
Merck index labeled? |
sorry , but i didn't get the meaning behind this
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holmes1880
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@Orbit,
You are right about the name. I found a whole lot more info on it, but synthesis is still a mystery. I did find a place to buy the pills though, so I
could potentially do some tests with it to see if its even worthwhile to make.
P.S. Don't pay attention to Wizard, he likes to troll far too often.
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TheOrbit
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there is no problem at all i tried to help only and i think we all try to help here.
if you see the manufacturing encyclopedia you will find this:
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The WiZard is In
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| Quote: Originally posted by TheOrbit |
| Quote: |
Trivia - What were the first few ed's of what is now called The
Merck index labeled? |
sorry , but i didn't get the meaning behind this
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The 1st 4 editions of what is now know as
The Merck Index were called Merck Index
Byda I posted this 12-1-2011 at 15:26
Synthsis is standard.
djh
----
I though for today.
I would paraphrase Haldane - God must have had an inordinate
fondness for carbon for he has made so many carbon compounds.
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