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Author: Subject: Potassium Trioxalato Ferrate III
vibbzlab
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Registered: 6-11-2019
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[*] posted on 6-11-2019 at 22:29
Potassium Trioxalato Ferrate III


I synthesised potassium Trioxalato Ferrate III . It's having this beautiful limegreen color to it. The points to note is that we should not keep it open in air as it decomposes.
I will give down the procedure I used to create it

1) Prepare a solution of 3.0 g of oxalic acid in 12.5mL of hotwater contained in a clean 50 mL beaker.

2) To the above solution, add 3.8 g of potassium hydroxidegradually in lots, with stirring so that it dissolves completely.

3)Add 2.5 g of ferric chloride into the above solution withconstant stirring till it is completely dissolved.

4)Filter the solution and concentrate the green filtrate byheating in a porcelain dish over a water bath and cool themixture slowly.

5)Filter the crystals so formed, wash with 1:1 mixture of coldwater and alcohol and dry them by pressing between thefolds of a filter paper.

I will also post down a link to the video where I synthesised it using the above procedure
https://youtu.be/_RruzgUHmjU

IMG_20191101_183123.jpg - 5.4MB
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