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Author: Subject: Strange P-nitroaniline color
stephill92
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[*] posted on 13-5-2020 at 14:36
Strange P-nitroaniline color


I recently purchased some p-nitro aniline off of amazon since it had good reviews and was fairly cheap, and upon receiving the package I noticed the chemical inside was black or dark blue. I tried melting it to see if it had a similar melting point to p-nitro aniline and it started to melt around 70c. At around 100c some yellow crystals started to appear on the side of the flask so I tried to pour off the black sludge and it formed some nice dark blue crystals when it cooled. I'm just curious if this has happened to anyone else since I know aniline and p-nitro aniline are prone to being oxidized but I wasn't expecting most of the sample I melted to be junk.
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DavidJR
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[*] posted on 13-5-2020 at 15:39


When pure it's very bright yellow, so I expect yours is significantly degraded - or perhaps just contaminated with something else entirely.
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