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Author: Subject: Uranium-Tungsten-Bismuth compound
vano
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[*] posted on 17-9-2022 at 04:28
Uranium-Tungsten-Bismuth compound


Hello! I made an unusual and rare compound, a heteropolymetalate containing Uranium, tungsten, and bismuth. here are some photos of the compound and structure. this is the formula Na13[Na(UO2)2(H2O)4(BiW9O33)2] * 33H2O.



Screenshot 2022-09-17 161712.png - 169kB
IMG-2344.jpg - 1.8MB
IMG-2345.jpg - 1.6MB




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Lion850
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[*] posted on 18-9-2022 at 00:26


Hi Vano very interesting. How did you make it?
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vano
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[*] posted on 18-9-2022 at 01:11


hello! that was easy, you need bismuth-tungsten heteropolymetalate and soluble uranyl salt. here is the paper, which contains also the synthesis of K&NH4 salts of this heteropolymetalate.



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[*] posted on 18-9-2022 at 01:16


Also if you want a methodic of synthesis of Na9[BiW9O33] *14H2O, just let me know, ill find it later. I made this as I made an antimony analog - Na9[α-SbW9O33]*27H2O.




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j_sum1
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[*] posted on 18-9-2022 at 03:05


Thanks vano. You always produce interesting stuff.
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[*] posted on 18-9-2022 at 03:16


thank you so much j_sum1!



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