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traumenz
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process for preparation of 2-methoxyethylbenzene
Hey guys!
I need process for the preparation of 2-methoxyethylbenzene
can any one help?
CAS Number : 3558-60-9
ESIS EC# (EINECS) :
222-619-7
Beilstein Number : 1857538
CoE Number : 11812
XlogP3 : 2.20 (est)
Molecular Weight : 136.19384000
Formula : C9 H12 O
Pherobase Floral: View
NMR Predictor : Predict
Category : flavor and fragrance agents
Synonyms :
chrysanthemum oxide
kedwa ether
kewda ether
1- methoxy-2-phenyl ethane
2- methoxyethyl benzene
(2- methoxyethyl) benzene
2- methoxyethylbenzene
methyl 2-phenethyl ether
methyl phenethyl ether
methyl phenethyl oxide
methyl phenyl ethyl ether
pandanol
phenethyl methyl ether
2- phenethyl methyl ether
phenyl ethyl methyl ether
2- phenyl ethyl methyl ether
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gutter_ca
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http://lmgtfy.com/?q=2-methoxyethylbenzene
[Edited on 7/31/2012 by gutter_ca]
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traumenz
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Thats not helping SIR!
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gutter_ca
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First result, jackass.
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Nicodem
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Thread Moved
1-8-2012 at 09:12 |
Hexavalent
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I like how this man has asked on at least 3 different chemical forums the same question, when a simple Google search would give him his answer.
[Edited on 1-8-2012 by Hexavalent]
"Success is going from failure to failure without loss of enthusiasm." Winston Churchill
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traumenz
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listen baby, im not good in chemistry, i need a methodology a simple one. keep quit if u cant help. if i was a good, i would be helping you instead!
take care!
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Hexavalent
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No, I won't email you directly as you asked in your little U2U to me.
Anyway, this chemical can be prepared by iodomethane and 2-phenyl-ethanol with metallic Na present. The reaction time is 2 hours with heating, and the
yield is about 42%.
Anyway, I wouldn't recommend someone who isn't 'good in chemistry' to do a synthesis like this.
But, to keep you quiet, I'd try taking the following procedure;
Dry some phenethyl alcohol thoroughly and prepare some fresh iodomethane.
Do some stoichiometry calculations for yourself, and work out how much of each you will need as well as an appropriate quantity for the sodium. Use
this to help you;
Chuck the lot into a RBF and reflux for 2 hours. Extract the product and characterize.
Just asking; a) are you in a professional lab, b) what qualifications do you have in chemistry, and c) what do you even want the product for?
*****
Reference; http://www.lookchem.com/2-Phenylethyl-methyl-ether/
[Edited on 1-8-2012 by Hexavalent]
"Success is going from failure to failure without loss of enthusiasm." Winston Churchill
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traumenz
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I would say thanks! Although you were rude. I’m not into chemistry. I’m masters in business administration. just helping some one out but not in a
lab. nothing more then that!
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Hexavalent
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No, I wasn't rude. It's just that we don't take kindly to people asking to be spoonfed information instead of searching for it themselves.
"Success is going from failure to failure without loss of enthusiasm." Winston Churchill
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traumenz
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forget it i dont want to make scores!
Well, according to your reaction the yield is 42% which is too low. I found a reaction it says, reacting phenyl ethyl alcohol with methanol in the
presence of sulphuric acid. Don’t know about the yield .
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Hexavalent
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Where is your reference for this?
P.S. Please don't be ignorant.
"Success is going from failure to failure without loss of enthusiasm." Winston Churchill
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traumenz
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great now you talk like a professional, I like that!
P.S I missed it 
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zoombafu
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The friend you are helping out better be good at organic chemistry and be able to get chemicals from suppliers. PEA isn't something you can find OTC.
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traumenz
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This benzene ring , I swear I feel like a prisoner in it ok, see I don’t have access to a journal called SYNTHETIC COMMUNICATION, 25,
page p2435 ,1995.there is much more detailed synthesis.
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traumenz
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No problem for PEA. i can get it.
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traumenz
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HONEY it say :
Error
Sorry, you are not permitted to view this forum
Sciencemadness Discussion Board » Error
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traumenz
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Hexavalent
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You know what? I've had enough of your complaning. I'll ask for you.
And stop referring to us as 'Baby' and 'Honey', please.
"Success is going from failure to failure without loss of enthusiasm." Winston Churchill
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Mailinmypocket
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Quote: Originally posted by traumenz  | HONEY it say :
Error
Sorry, you are not permitted to view this forum
Sciencemadness Discussion Board » Error |
That is because you need to ask admin for access, which is usually granted after being a member on the forum for a while and contributing to
discussions.
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traumenz
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| Quote: Originally posted by Hexavalent | You know what? I've had enough of your complaning. I'll ask for you.
And stop referring to us as 'Baby' and 'Honey', please. |
lolz, ok, sure! love u! thanks again!
come on man, its just i've in my mind that i am in a professional forum and some people might help and they are help full.i can see that. dont mind
dear!
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Mailinmypocket
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Is something wrong with you? If you have in your mind that you are in a professional forum then try not using pet names and telling people
things like "love you" and ending posts with "dear"
It just looks plain stupid and childish and makes others even less tempted to help you.
Oh and do try and use proper spelling, punctuation and all the other goodies you would expect in a "professional" environment.
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zoombafu
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If you want to be professional don't call people baby.
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Hexavalent
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Unless you happen to be a professional whore
I have to agree with these guys, though - we welcome newcomers, as long as they make some effort to "fit in", i.e. by making useful posts, maintaining
a standard of professionalism and using correct spelling, punctuation and grammar.
[Edited on 1-8-2012 by Hexavalent]
"Success is going from failure to failure without loss of enthusiasm." Winston Churchill
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traumenz
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hahahahaha, ok when you don't have any thing to help in chemistry you are correcting English. this should be a grammar forum.
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traumenz
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bunch of chotia's around here!
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