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RIPPER
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wink.gif posted on 25-9-2004 at 03:28
Caros Acid

Are Caros Acid (H2SO4 + H2O2) a good oxidizer for a amino group ?
When the starting material dissolved in concentrated H2SO4
an than added the H2O2.
I have idea to make high percent H2O2, when the
normal H2O2 dissolved in acetic anhydride and than
added dropvise to the mix ?

:cool::mad:
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BromicAcid
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[*] posted on 25-9-2004 at 16:04


Yes, Caros acid is a good oxidizer for the amino group, as a matter of fact it can be used for the conversion of pentanitroanaline to hexanitrobenzene.



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unionised
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[*] posted on 26-9-2004 at 14:43


Reaction of H2O2 and acetic anhydride can give peracetic acid, which is nasty and acetyl peroxide which is worse.
Adding this to sulphuric acid and an organic reducing agent isn't a reaction I would want to do.
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[*] posted on 27-9-2004 at 05:05


Isn't H2SO4+H2O2 known as "piranha solution" for its ability to chew away organics? Including flesh?
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[*] posted on 27-9-2004 at 10:54


the frightener



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RIPPER
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mad.gif posted on 28-9-2004 at 04:15
high nitrated

Are high nitrated nitro anillines (phenols, anisols) not instable and high water soluble ?
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[*] posted on 30-9-2004 at 04:58
anilline

I believe Trinitroaniline is a real makeable
energetic material.

:(
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[*] posted on 2-10-2004 at 17:00


Just made "pirahna acid" and it rightfully deserves that name! I mixed excess h2so4 with 30% h2o2, and palced a small amoutn (like 5 ml) on this 1/8th thick opeice of cardboard...stuff ate right through it like 5 seconds. Everything began to smoke and smell of SOx im guessing... cool stuff. I'd be careful with it though as I don't want to what it'd do the the flesh.... It's a claerish liquid with a pinkish tint maybe.
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