PariahParadox
Harmless
Posts: 3
Registered: 15-9-2014
Member Is Offline
Mood: No Mood
|
|
Hexamine Synthesis
Hello, I am new to this forum, and while I don't have the glassware, I am very interested in the synthesis of Hexamine.
I did locate some books in the library section of Sciencemadness and few others on the Internet, but I would still
like to read about a more detailed lab synthesis paper before attempting it myself.
I did see the synthesis thread here on sciencemadness: http://www.sciencemadness.org/talk/viewthread.php?tid=3229#p...
Also this video was pretty informative: https://www.youtube.com/watch?v=d2N0zAoVYew
What I am trying to find is a more detailed synthesis of hexamine from a good laboratory organic chemistry book
so I can read it on my own time.
Thanks in advance.
[Edited on 19-9-2014 by PariahParadox]
|
|
|
TheChemiKid
Hazard to Others
Posts: 493
Registered: 5-8-2013
Location: ̿̿ ̿̿ ̿'̿'̵͇̿̿з=༼ ▀̿̿Ĺ̯̿̿▀̿ ̿ ༽
Member Is Offline
Mood: No Mood
|
|
It's a pretty straightforward synthesis, why do you need to book?
|
|
|
PariahParadox
Harmless
Posts: 3
Registered: 15-9-2014
Member Is Offline
Mood: No Mood
|
|
I do have a tendency to second guess myself and I do have a link to another video: https://www.youtube.com/watch?v=mCCpl08_WjQ where this guy actually does not use lab glassware or an ice bath and says that it smells strongly of
ammonia.
I want to do it the safe way but I feel better looking at information that I know I can trust like the Journal of American Chemical Society.
I realize that the synthesis is basic I am just surprised that there is no modern day book detailing its synthesis unless I go back in the library
section of sciencemadness and I did find at least one book pdf file with some info - s-Triazines and Derivatives (The Chemistry of Heterocyclic
Compounds, Volume 13).
|
|
|
violet sin
International Hazard
Posts: 1475
Registered: 2-9-2012
Location: Daydreaming of uraninite...
Member Is Offline
Mood: Good
|
|
the first link on the opening post, is missing a "g" in "madness.org". I had to type it into the address bar after the link failed to load for me
several times.
|
|
|
PariahParadox
Harmless
Posts: 3
Registered: 15-9-2014
Member Is Offline
Mood: No Mood
|
|
Quote: Originally posted by violet sin  | the first link on the opening post, is missing a "g" in "madness.org". I had to type it into the address bar after the link failed to load for me
several times.
|
Fixed. Thank you for letting me know.
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
