Quince
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Nepetalactone extraction
I attempted to extract the essential oil from catnip in a Gregar extractor using ethanol as the solvent. Unfortunately, the high boiling temperature
of the ethanol resulted in some burning along the boiling flask.
Some questions:
The most common solvent for extracting essential oils from aromatic plants seems to be hexane. However, I don't see where I can obtain this OTC. Any
appropriate substitutes? One I've seen mentioned occasionally is methylene chloride.
Another thing is, how do I separate out various things the solvent took along from the oil? The ethanol extracted most of the chlorophyll. And
hexane extracts a lot of waxy substances besides oils.
\"One of the surest signs of Conrad\'s genius is that women dislike his books.\" --George Orwell
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leu
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Chromatography is the normally used technique for such separations 
Chemistry is our Covalent Bond
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runlabrun
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you would normally extract with some solvent (hexane or whatever) then distill off the solvent to obtain the residual gum and fractionally distill
this under hard vacuum to obtain whatever fraction you want.
-rlr
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Twospoons
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"White gas" or "White spirit" , as used in liquid fuelled camp stoves, is mostly n-Hexane.
Helicopter: "helico" -> spiral, "pter" -> with wings
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Quince
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Twospoons, white gas/spirit, according to the Web, is a mixture of a whole bunch of stuff, and only some limited percentage is hexane. With my luck,
it probably forms azeotropes with some of the other ingredients.
[Edited on 18-2-2006 by Quince]
\"One of the surest signs of Conrad\'s genius is that women dislike his books.\" --George Orwell
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leu
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Obviously some posters are taught differently than others have been. Attempting to reinvent the wheel is rather inefficient, library research is often
more productive in finding the already published procedure  This problem was
solved at the University of Wisconsin many years ago, the paper on the isolation of nepetalic acid, nepelactone and related compounds has been
uploaded to the Wet Dreams thread for literature requests from this and other forums
[Edited on 19-2-2006 by leu]
Chemistry is our Covalent Bond
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Quince
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I'm unable to access the site.
Why do you have to be so difficult and not at least post the citation, so I can at least find the paper myself?
\"One of the surest signs of Conrad\'s genius is that women dislike his books.\" --George Orwell
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Quince
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In the attached 2005 paper, under traditional method (procedure B in the experimental section), they extract with methylene chloride the water from
the mincing, and the solid stuff, separately. Why???
Also, where do I get the silica for method A? It's not clear to me from the description exactly how to perform this method. Anyone care to propose a
DIY method?
Attachment: np049647d.pdf (132kB)
This file has been downloaded 1458 times
\"One of the surest signs of Conrad\'s genius is that women dislike his books.\" --George Orwell
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