idrbur
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is distillation required?
I want to make aniline from indigo. There 2 methods for this.in first method destructive distillation of indigo is performed but in 2nd method KOH
and indigo are mixed .so i want to know does distillation also required in 2nd method?
And i also want to know that what are the products in both reactions.
[Edited on 13-7-2015 by idrbur]
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Bert
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Thread Moved
13-7-2015 at 09:51 |
Bert
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Mood: " I think we are all going to die. I think that love is an illusion. We are flawed, my darling".
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idrbur:
Posting FAQ:
http://www.sciencemadness.org/madscifaq.html#2.1_Board_topic...
The short question thread in "Miscelaneous":
https://www.sciencemadness.org/whisper/viewthread.php?tid=25...
Short question, quick answer thread for energetic materials:
https://www.sciencemadness.org/whisper/viewthread.php?tid=26...
Please confine your posts to "beginnings" or the "short question, quick answer" threads- Unless you take time to provide links or quotes of materials
related to your questions, and/or descriptions of your lab work related to process and questions being posted.
I (and many others!) like that you are interested in chemistry, but a little discipline in posting will make everyone more interested in answering
you!
Rapopart’s Rules for critical commentary:
1. Attempt to re-express your target’s position so clearly, vividly and fairly that your target says: “Thanks, I wish I’d thought of putting it
that way.”
2. List any points of agreement (especially if they are not matters of general or widespread agreement).
3. Mention anything you have learned from your target.
4. Only then are you permitted to say so much as a word of rebuttal or criticism.
Anatol Rapoport was a Russian-born American mathematical psychologist (1911-2007).
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aga
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Do you have any links to those two procedures ?
Distillation is generally a great thing to be able to do, as it is useful for many experiments.
Whether you distill water out of it or not, it's going to smell horrible !
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idrbur
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This is the link-
https://en.m.wikipedia.org/wiki/Aniline
But on this there is not much information about procedure.
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idrbur
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This is the link-
https://en.m.wikipedia.org/wiki/Aniline
But on this there is not much information about procedure.
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aga
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Yes, there isn't a great deal of info there.
It says that "Fritsche 'treated' indigo with KOH ... and obtained an oil ..."
If you have Indigo and KOH, do a few small scale experiments (test tube size) to find the best procedure.
All you're looking for is an isolatable oil that stinks of dead fish.
Distillation will be for purifying it.
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idrbur
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Thanks for reply aga.
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idrbur
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Thanks for reply aga.
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