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Author: Subject: Thermometer choice
glassplass
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[*] posted on 16-3-2016 at 12:08
Thermometer choice


Hi folks!
I need quick help.
Which thermometer is better to use in distillation aparatus,total or partial immerised?
The thing is little bit confusing.
I thing 76mm partial immerised is good option but i am not sure.
Please help! :D
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aga
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[*] posted on 16-3-2016 at 12:14


yes, you are right.
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arkoma
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[*] posted on 16-3-2016 at 12:33


This is a good question. Shit confuses me too, and I don't even KNOW what my chinese thermometers are--no markings. Blogfast, can ya weigh in and enlighten us perhaps?



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S.C. Wack
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[*] posted on 16-3-2016 at 14:30


Never buy a total immersion thermometer unless you need one.

Check your thermometers for a line aound them at a certain distance from the bulb.




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Dr.Bob
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[*] posted on 16-3-2016 at 16:23


For most distillations, you typically want a 1-3" immersion thermometer, so the vapors are covering the part from the bulb to the line. Depends on the particular distillation head, and the length of it.
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Sulaiman
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[*] posted on 17-3-2016 at 04:43


AFAIK if there is no line or text to indicate immersion level then it is a total immersion thermometer.
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j_sum1
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[*] posted on 17-3-2016 at 04:52


In practice, how much difference will it make?
The column is a small fraction of the total volume. I can't imagine that it would throw out the reading at a significant level for most applications.




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DJF90
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[*] posted on 17-3-2016 at 05:17


There are stem corrections you can apply to a total immersion thermometer that is being used for partial immersion.

See here (at the bottom of the page)
http://www.coleparmer.co.uk/TechLibraryArticle/670

EDIT: Also see attached paper

[Edited on 17-3-2016 by DJF90]

Attachment: A nomograph for emergent stem correction of thermometers.pdf (87kB)
This file has been downloaded 284 times

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[*] posted on 17-3-2016 at 06:00


Thanx DJF, between the link and the nomograph I can begin to make some sense of this. Vogel's Third was a bit obtuse for me.



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DistractionGrating
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[*] posted on 17-3-2016 at 07:11


There is this link too: http://www.icllabs.com/thergenlinfo.html
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chemrox
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[*] posted on 17-3-2016 at 11:13


Thanks DJF90- I printed and posted in my lab.



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chemrox
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[*] posted on 17-3-2016 at 17:42


I like properly marked Hg thermometers. US or German made..



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