Metacelsus
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Second-order NMR splitting
Can anyone identify this pattern? It showed up in the spectrum of a side product of one of my reactions, and I haven't seen anything like it before.
(The spectrum was taken in CDCl3 at 400 MHz).
Edit: These peaks are almost certainly from 2 different compounds.
[Edited on 12-10-2016 by Metacelsus]
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Eddygp
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I was expecting a doublet of a doublet... but this.. Wow!!
H MNR I guess, yes?
Is there any F, P or some other NMR active element in your sample? (apart from H, but that can couple to H)
there may be bugs in gfind
[ˌɛdidʒiˈpiː] IPA pronunciation for my Username |
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Metacelsus
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No, it's just H, C, O, and S. I'm starting to think that it might just be two unrelated pairs of doublets from an impure sample.
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DJF90
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Sure looks that way
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Metacelsus
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Yes, it's definitely at least 2 compounds. Originally, it was 1 peak on the MPLC, but I changed to a better eluent, and it came off as 2.
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DJF90
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Glad to hear you resolved the issue.
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