sulfuric acid is the king
Hazard to Self
Posts: 94
Registered: 11-1-2017
Member Is Offline
|
|
Small scale dehydrogenation
I think and hope it's not double post.
Does anybody have idea how can it be done?I do not have Pd,Pt,etc...
|
|
|
Nicodem
|
Thread Moved
5-3-2017 at 13:53 |
Nicodem
|
Thread Moved
5-3-2017 at 13:54 |
Eddygp
National Hazard
Posts: 858
Registered: 31-3-2012
Location: University of York, UK
Member Is Offline
Mood: Organometallic
|
|
It probably depends a lot on what system you are trying to dehydrogenate. There were these articles...I think that it was for systems that yield a
conjugated product, I remember having found a lot of information about using selenium (if I remember correctly, elemental) with very decent yields.
there may be bugs in gfind
[ˌɛdidʒiˈpiː] IPA pronunciation for my Username |
|
|
sulfuric acid is the king
Hazard to Self
Posts: 94
Registered: 11-1-2017
Member Is Offline
|
|
Linear alkanes.
|
|
|
Zandins
Harmless
Posts: 25
Registered: 18-6-2016
Member Is Offline
Mood: No Mood
|
|
As far as I understand, you want to remove 2 hydrogens from an alkane to form a double bond?
Alkanes are generally unreactive, so your best bet is probably a free radical halogenation, followed by an elimination reaction to give the alkene.
However, the halogenation will give a mixture of halogenated compounds, which may be difficult to separate.
What exactly do you want to make and from what? Some specifics would be very helpful.
[Edited on 8-3-2017 by Zandins]
|
|
|
Texium
Administrator
Posts: 4508
Registered: 11-1-2014
Location: Salt Lake City
Member Is Offline
Mood: PhD candidate!
|
|
Probably drugs. I feel
like this is going to end up in detritus whether or not the OP provides more information...
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
