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Author: Subject: Chromium Sulphate from Stainless Steel
mesanaw
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[*] posted on 28-6-2017 at 15:47
Chromium Sulphate from Stainless Steel


I'm trying to make Chrome Alum from stainless steel as a starting material, but I am having trouble separating chromium sulfate from the ferrous sulfate.

The resulting mixture from reacting stainless steel with dilute sulfuric acid is two parts: one is a dark liquid and the other a green slushy-like material. The dark liquid portion clearly has some ferrous sulfate in it.

Is there any way to separate the two compounds while leaving the chromium sulfate in tact?
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DraconicAcid
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[*] posted on 28-6-2017 at 15:49


Isolation of chromium compounds from stainless steel has been discussed in other threads.

I suggest sodium hydroxide. Cr forms a soluble complex ion; Fe does not.




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