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Author: Subject: proprionic anhydride new rt synthesis
spankyetal
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[*] posted on 30-8-2017 at 20:18
proprionic anhydride new rt synthesis


was pleasantly surprised to discover a fairly new synthesis for the dehydration of proprionic acid to the anhydride, carried out at room temp, actually worked. Yield was within 1% of predicted.
As a disclaimer I must state that at no time did any activities described herein take place within the jurisdiction of the United States, its territories, or treaty lands. The catalyst involved was a challenge to make to say the least. Many new pieces of lab equipment had to be created thus adding to the fun of creation. Not quite sure as what to do with the materials, methods, and gobs -so scientific yes!- of product involved.
An illustrated and informative CD perhaps.
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Crowfjord
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[*] posted on 31-8-2017 at 13:21


Any details on that, or maybe a reference? Also propionic anhydride is not illegal in the US, so the disclaimer is superfluous.
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phlogiston
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[*] posted on 1-9-2017 at 00:52


What is the point of your post? There is no information in it, not even an idea or plan, nor any questions.



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"If a rocket goes up, who cares where it comes down, that's not my concern said Wernher von Braun" - Tom Lehrer
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gdflp
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1-9-2017 at 08:27
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[*] posted on 1-9-2017 at 08:30


For now, this is going to Detritus, since there is no useful information in it whatsoever.

Also, posts with a "disclaimer" are not allowed on SciMad, they're just as bad as SWIM posts.




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