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Author: Subject: Issues with Soxhlet set up
JJay
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[*] posted on 19-1-2018 at 16:15


I think you're making mescaline.



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NEMO-Chemistry
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[*] posted on 19-1-2018 at 21:42


I think your better buying it, cheaper, much quicker. Your way isnt going to work well, i dont think your Mescaline like that though, i think your aiming for black tar crap. But JJay could be right, it could be Mescaline, but me thinks i got him this time! I am 99.9% sure your target with that method is black crap.

Oh and a nice warm house......If your skint how come you can afford a very large amount of ether your going to use?

[Edited on 20-1-2018 by NEMO-Chemistry]
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S.C. Wack
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[*] posted on 20-1-2018 at 09:37


I think he's making people react. If he actually had the nitrostyrene, ether, and LAH, the target is fire.



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[*] posted on 20-1-2018 at 10:25


He's gonna use dry ice and a Graham condenser for ether???
Don't think this poster is exactly lab-savvy.
Don't think he's ever used either ether. (Used ether either, sorry.)

But isn't the point of this modification so you can use less ether to dissolve reactants for the reaction?

If just adding a saturated solution really slowly is all you're after, then break out one of those constant addition funnels.
Those suckers are just worlds apart from regular pressure compensating addition funnels for this kind of thing.




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S.C. Wack
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[*] posted on 20-1-2018 at 11:37


Check the original literature of Ramirez and Burger, and Nystrom and Brown, which is on Rhodium and elsewhere. The pressure equalizing funnel I mentioned earlier is for the side arm which is much like the Soxhlet's.



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