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Author: Subject: Oxalyl Chloride Challenge
Keras
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[*] posted on 9-7-2022 at 02:39


Did anyone try the method, described in a Chemplayer’s video, of making acyl chlorides by passing dry HCl into an ice-chilled mixture of acetonitrile and said carboxylic acid (in this case, oxalic acid)?
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ErgoloidMesylate
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[*] posted on 19-8-2022 at 10:13


Quote: Originally posted by Praxichys  
Well, beans. Back to the drawing board.


Incredible.
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[*] posted on 19-8-2022 at 10:23


Quote: Originally posted by Keras  
Did anyone try the method, described in a Chemplayer’s video, of making acyl chlorides by passing dry HCl into an ice-chilled mixture of acetonitrile and said carboxylic acid (in this case, oxalic acid)?


Looks to me like the only sure way of doing it is with phosphorus pentachloride, sorry.
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