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Author: Subject: Last chemical order?
Kaifas
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[*] posted on 4-2-2008 at 07:36
Last chemical order?


Mine is here - 13 bottles of ACS grade chemicals. What is yours?

chemicals.jpg - 290kB
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YT2095
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[*] posted on 4-2-2008 at 07:42


500g sodium nitrite
500g Ammonium Bifluoride
100g sodium hypophosphite.




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SecretSquirrel
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[*] posted on 4-2-2008 at 08:44


1L acetic acid, 1kg ammonium sulfate, 250g NaBr, 250g sodium acetate and Dimroth condenser with 50 cm jacket :)
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Aikimike
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[*] posted on 4-2-2008 at 09:50


250g.Na2SO4
100g. Boric Acid
100g., Stearic Acid
500g. Na Benzoate
1,2 Dichlorobenzene 100ml
1,3 Dichlorobenzene 100ml
1,4 Dichlorobenzene 50g
100g. CuOCl
500ml. Anhydrous Ethanol
500g. Na metal
1l. Methylene Chloride
500g. Sodium Dichromate
500g. Pentarythritol
50g. Na2S2O3
100g. I2
100g. Mercury metal
100ml. Universal Indicator liquid
500ml. Nitrocellulose solution
250g. Anti bumping Granules
250g. Anhydrous Sodium Carbonate
Decane 100ml
Hexachlorobutadiene 500ml
Cyanoacetic acid 250g.
500g. K2CO3
1000ml. Hexane
500g Oxalic Acid
250g Hydroquinnone
250g Ammonium Acetete
terephtalaldehyde
5-bromo-2methoxybenzaldehyde
2kg phenol
MnO2
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YT2095
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[*] posted on 4-2-2008 at 10:01


Quote:
Originally posted by Aikimike
250g.Na2SO4
100g. Boric Acid
100g., Stearic Acid
500g. Na Benzoate
1,2 Dichlorobenzene 100ml
1,3 Dichlorobenzene 100ml
1,4 Dichlorobenzene 50g
100g. CuOCl
500ml. Anhydrous Ethanol
500g. Na metal
1l. Methylene Chloride
500g. Sodium Dichromate
500g. Pentarythritol
50g. Na2S2O3
100g. I2
100g. Mercury metal
100ml. Universal Indicator liquid
500ml. Nitrocellulose solution
250g. Anti bumping Granules
250g. Anhydrous Sodium Carbonate
Decane 100ml
Hexachlorobutadiene 500ml
Cyanoacetic acid 250g.
500g. K2CO3
1000ml. Hexane
500g Oxalic Acid
250g Hydroquinnone
250g Ammonium Acetete
terephtalaldehyde
5-bromo-2methoxybenzaldehyde
2kg phenol
MnO2


where did you purchase all that from in one order?




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Kaifas
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[*] posted on 4-2-2008 at 10:17


Nice order!

Here is the list

All from Scharlau

500g. Potassium Chlorate
500g. Potassium Perchlorate
500g. Sodium Perchlorate
1000g. Sodium Chlorate
1000g. Potassium nitrate
500g. Potassium carbonate
500g. Sodium nitrate
500g. Strontium nitrate
500g. Barium nitrate
100g. Cu(II)chloride
100g. Cu(I)cyanide
500g. Copper(II)sulfate pentahydrate
250G. Copper powder
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kaviaari
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[*] posted on 4-2-2008 at 10:19


2,5l of HPLC grade methanol
100g of iodine
500g of anh. sodium sulfate
1kg of sodium hydroxide
100g of magnesium flakes
100g of pure sodium
1l of acetyl chloride
250g of benzophenone
250ml of brombenzene
1l of MTBE

I have been working with Gringard reactants. Which is somewhat clear when you go through the list.
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YT2095
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[*] posted on 4-2-2008 at 10:22


Evidently Pyro uses in mind for those then?

although I think If I were going to be using it for Pyro I`d lose the sodiun nitrate and chlorate and get some Am Perc instead;)




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microcosmicus
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[*] posted on 4-2-2008 at 10:29


Unfortunately, where I am located (U.S.) buying a bunch of ACS grade
chemicals from a proper supplier is out of the question for reasons
thoroughly discussed in the legal issues forum :( My last purchase
was from the local ceramic supply store:

BaCO3
MnO2
TiO2
SiO2

In the meanwhile, I picked up some HCl and similar odds and ends
from the hardware store.

[Edited on 4-2-2008 by microcosmicus]
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Aikimike
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[*] posted on 4-2-2008 at 10:37


Ah, do Scharlau supply to private individuals?

YT2095, if you would like info on my supplier P.M. me please.
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Kaifas
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[*] posted on 4-2-2008 at 10:46


Sodium salts dissolves much better than potassium salts so it is reason to use both potassium and sodium. I use oxidizers to do some Copper perclorate (binds strongly to nitrogen bases) and copper(III) compounds and making different copper complexes . Copper(I)cyanade goes to Gillman reagents. Copper(II)chloride is starting material to do Glacer couplings. Copper powder goes to Ullman coupling reactions.

Sodium nitrate is exellent for mild nitration systems because of good solubility.

It is difficult to byu chemicals here too.
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[*] posted on 4-2-2008 at 10:58


Quote:
Originally posted by Aikimike
Ah, do Scharlau supply to private individuals?

YT2095, if you would like info on my supplier P.M. me please.

You can actually order from about every company you want. But be smart. Find an intermediate supplier, who sells to individuals, and as him to buy for you. They are a company and can order from such companies. My acids / solvents are from Acros/Baker/Fisher, and Im no company or school! I don't lie , look in Tour My Lab!
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Aikimike
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[*] posted on 4-2-2008 at 11:12


I know what you mean Jor. Its definaltely something that I am trying to look into but the main issue is that very few people are willing to act as an intermediate!

There is no doubt that I prefer chemicals from very well known companies, but I settle for getting everything I need from slightly less well known places :)

Thanks alot
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[*] posted on 4-2-2008 at 11:29


1l p.a. toluene
1l p.a. 36% formaldehyde
1l p.a. methyl ethyl ketone




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[*] posted on 4-2-2008 at 13:04


1kg sodium hydroxide
500g sodium dichromate
1kg calcium chloride
1L acetone
1L methanol

*bullshit deleted*

[Edited on 6-2-2008 by organometallic]




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Aikimike
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[*] posted on 4-2-2008 at 13:36


I didn't know YT2095 had any 5-bromo-2methoxybenzaldehyde :)

I'll be honest, it was offered to me very cheaply so I decided that I'd get ahold of some, and then ironically post here to see what people thought to do with it.

I am getting 20g. only though...

Before anyone gets any ideas about some of the stuff there... I have absolutly no intentions whatsoever of doing anything illegal. I am just facinated by chemistry.
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MadHatter
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[*] posted on 4-2-2008 at 20:03
Chemical Order


Chlorowax, saran, strontium carbonate, air float charcoal, sodium benzoate - all pyro.



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YT2095
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[*] posted on 5-2-2008 at 01:09


Quote:
Originally posted by organometallic

YT2095, sorry for being nosy, but do you intend to react the 5-bromo-2methoxybenzaldehyde with nitroethane?


those aren`t mine, in fact I have very little in the way Organic chems here, and certainly no complex organics unless you count Metol the photo developer :)




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organometallic
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[*] posted on 6-2-2008 at 06:50


YT; Aikimike
Soz, stupidity on my part, i thought it was YTs.
Fair enough, its always better to stay legal.
Anyway i was talking shit.
OM




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Aikimike
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[*] posted on 6-2-2008 at 16:39


Don't worry about it Organometallic!

And yes, I shall be staying on the right side of the law! No nitrostyrenes of 2,5 Dimethoxybenzaldehyde!
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[*] posted on 6-2-2008 at 21:30


Myself,
Magnesium Turnings and Palladium (II) Chloride
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Kaifas
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[*] posted on 7-2-2008 at 10:18


Palladium(II)chloride? Sounds like coupling reactions....

--Kaifas
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[*] posted on 7-2-2008 at 11:00


One gram each of the (III) chlorides of Ru, Ir, Os, Re, Rh. Not out of my pocket.

[Edited on 7-2-2008 by Swany]
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[*] posted on 7-2-2008 at 11:29


Quote:
Originally posted by Kaifas
Palladium(II)chloride? Sounds like coupling reactions....

--Kaifas


I got it because it was very under priced. :D
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[*] posted on 16-2-2008 at 20:05


Mine isn't nearly as chemically exciting as most of your guys'. I got a 55lb bag of soluble glutonous rice starch the other day. 10lbs of Titanium sponge not to long before that. That is assuming you don't count the lactic acid and burton salts I picked up yesterday at the home brew shop as chemical purchases. Not much pure chemistry for me as of late.
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