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Schleimsäure
Hazard to Others
Posts: 156
Registered: 31-8-2014
Location: good ole Germany
Member Is Offline
Mood: Probably
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Will collect a big order in a few days:
1,4-Dioxane 2l
1,10-Phenantroline 100g
1-Pentanole 1l
1-Propanole 2l
4-Aminobenzoicacid 100g
4-Nitrophenole 250g
Acetaldehyde 500 ml
Acetylchloride 85 ml
Adipinic acid 250g
Alkali blue 50g
Ammoniumdichromate 500g
Ammoniummolybdate 100g
Anthracene 250g
Antimonpentachloride 250 g (>100 ml)
Arsene (III)-oxid 250g
Bismuthchloride 50g
Lead(II)-acetate 250g
Lead(II)-chloride 100g
Lead(II)-nitrate 1 kg
Bromothymoleblue 50g
Cer(IV).oxide 100g
Chloralhydrate 328 g +164 g
Benzoylchloride 1,64 L
Cyclohexanole 3l
Diphenylamine 250 g
Ferrous (III)-chloride anhydrous 500g
Formamide 500ml
Hexachloroethane 1 kg (technical)
Hexachlororethane 1 kg (pure)
Hydrazinesulfate 500g
Hydrochinone 250g
Hydroxylamine HCl 500g
Iodinechloride 50g
HI 55% 100ml
Potassiumbromate 250g
Carbondisulfide 2l
Kresolered 50g
Lanthaniumchloride 25g
LiAlH 150g
Malachite green 50g
Malonic acid 250g
Chloroacetic acid 2 kg
Sodium azide 250g
Sodium sulfide 1 kg
n-Butanole 2l
Nitrobenzene 1l
Paraformaldehyde 326 g
Periodic acid 100 g
Phenyleacetic acid 500 g
Pyrogallole 250g
Propionic acid 1l
Pyrrole 50ml
Rhodamine B 50g
Nitric acid >98% 1l
Triethanoleamine 1l
Triflouroactic acid 100 ml
Uranylacetate 25g
Stannic chloride 5xH2O 100g
Chlorobenzene 1l
Resorcine 1kg
Thiourea 1kg
Sodium 1 kg
Aluminum(III)-chloride anh. 500g
Copper(II)-chloride 250g
Acetonitile 1 L
Cadmiumchloride 250 g
Maybe I can give away smaller amounts (50 to 250 g or ml), if it's within the law of the respective country. Only two items are technical grade, rest
is pure at least.
[Edited on 15-10-2016 by Schleimsäure]
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CharlieA
National Hazard
Posts: 645
Registered: 11-8-2015
Location: Missouri, USA
Member Is Offline
Mood: No Mood
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urea, benzoic acid, oxalic acid, EDTANa2
for mp standards and future syntheses
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Brom
Hazard to Self
Posts: 94
Registered: 19-7-2015
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Mood: No Mood
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j_sum1
Administrator
Posts: 6219
Registered: 4-10-2014
Location: Unmoved
Member Is Offline
Mood: Organised
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Not sure what I am going to do with it. But it seemed too good to pass up. I am going to recommend the seller: there are a lot of interesting
product lines and all seem to be at a reasonable price. A good source for Aussies in particular who are after natural extracts and food-related
products.
www.stores.ebay.com.au/AXENIC-Labs
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wg48
National Hazard
Posts: 821
Registered: 21-11-2015
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Mood: No Mood
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Quote: Originally posted by AngelEyes  | Darrant Chemicals - anyone had any dealings with them?
I ordered some bits on the 20th Sept, nothing dodgy or nasty, but have had nothing back. They took the cash immediately, but then squat. No delivery,
no emails, no phone calls and if you try to call them it just rings and rings. Found this:
https://www.yell.com/biz/darrant-chemicals-lincoln-8313838/
...which does not fill me with confidence.
I'll give it another few days but then, assuming I have still got nothing, I may have to write it off. Annoying. I'd not recommend these cowboys at
all.
I used a credit card...anyone know my rights on getting a refund etc?
Cheers
Angel. |
Have you received your order ? Have they responded to you?
I was considering ordering from them but perhaps not anymore.
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woelen
Super Administrator
Posts: 7976
Registered: 20-8-2005
Location: Netherlands
Member Is Offline
Mood: interested
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I had a nice exchange last week.
10 grams of 99.9999% arsenic, ampouled in glass under argon, an ampoule full of Be (99.9%) and a disk of Be 99.9% (4 cm x 3 mm) in exchange for 4
ampoules, filled with NO2 gas and 2 ampoules filled with BrCl. I made these ampoules with the gasses myself. I have a few very beautiful samples added
to my element collection 
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j_sum1
Administrator
Posts: 6219
Registered: 4-10-2014
Location: Unmoved
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Mood: Organised
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Not a chemical order -- do we have one of these threads for hardware?
I am not pretending that it is going to be high quality but at the price is was worth grabbing.
http://www.ebay.com/itm/311616125799
The downside is that I am sure that customs/police will interpret it as some kind of dope bong and the boys in blue will pay me another visit. And I
will have to justify the existence of my lab yet again [sigh].
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CharlieA
National Hazard
Posts: 645
Registered: 11-8-2015
Location: Missouri, USA
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Mood: No Mood
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Nice piece of glassware!
Why are so many members of this board so paranoid?
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j_sum1
Administrator
Posts: 6219
Registered: 4-10-2014
Location: Unmoved
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Mood: Organised
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Because I have had a coupe of visits from ordering Chinese glassware and having it intercepted at customs.
The first visit was friendly enough. The second was a bit nasty and my item was confiscated. (Although I was answering all their questions as
accurately as I could, I was describing a Dean Stark that I had on order and not the drying tube that they had stalled at customs. Because I had not
correctly identified the item they apparently decided that I had no legitimate use for it.) In short, I am becoming familiar with the systems in use
around here and know that the cow adapter may cause headaches. But at fifteen bucks it is worth the risk.
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NedsHead
Hazard to Others
Posts: 409
Registered: 9-12-2014
Location: South Australia
Member Is Offline
Mood: No Mood
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if I recall correctly you said you're a school teacher J? and even with that knowledge the police still give you the 3rd degree?? I find that really
shocking!, announcing you are a teacher and giving them a tour of your lab should be enough to have them treat you respectfully and leave you alone
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j_sum1
Administrator
Posts: 6219
Registered: 4-10-2014
Location: Unmoved
Member Is Offline
Mood: Organised
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You have it correct NH. But this is not the thread for this discussion. I might fill in details in Tdep's "Police finally showed up" thread.
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CharlieA
National Hazard
Posts: 645
Registered: 11-8-2015
Location: Missouri, USA
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Mood: No Mood
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Not a chemical order, but related...My wife an I attended a flea market in Grafton, IL a week or so ago. I make stuff with a scroll saw, and even
though I am somewhat (snobbishly) disdainful of those who make stuff with a computer-guided laser/router/wood burning stylus, etc., she found this for
me. It is made on a sheet of 3/16" thick x ~17" high x ~24" wide plywood. I would certainly have been driven crazy (crazier?) trying to make something
similar on my scroll saw. Now I just have to make a suitable frame for it...
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mayko
International Hazard
Posts: 1218
Registered: 17-1-2013
Location: Carrboro, NC
Member Is Offline
Mood: anomalous (Euclid class)
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| Quote: Originally posted by mayko | It wasn't expensive so I got a pack but I haven't come up with a good way to separate the silicate from the carbonate and others. I wonder if I can
grow a chemical garden in it?
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I made a strong solution and let it cool, then poured off the supernatant from the crystals which formed. This is indeed generating tubes and spikes
from some nickel/cobalt salts i threw in!
al-khemie is not a terrorist organization
"Chemicals, chemicals... I need chemicals!" - George Hayduke
"Wubbalubba dub-dub!" - Rick Sanchez
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brubei
Hazard to Others
Posts: 187
Registered: 8-3-2015
Location: France
Member Is Offline
Mood: No Mood
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I'm about to send little order to a shop (nov. 21th)
Graphite
SiO2 40-60 µm
CaSO4
Pissette
KOH
I can share those with someone in EU.
They also have a huge catalogue if you can't access to some products for any reason, except schedule compounds
[Edited on 9-11-2016 by brubei]
[Edited on 10-11-2016 by brubei]
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CharlieA
National Hazard
Posts: 645
Registered: 11-8-2015
Location: Missouri, USA
Member Is Offline
Mood: No Mood
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I forgot the picture!
| Quote: Originally posted by CharlieA | Not a chemical order, but related...My wife and I attended a flea market in Grafton, IL a week or so ago. I make stuff with a scroll saw, and even
though I am somewhat (snobbishly) disdainful of those who make stuff with a computer-guided laser/router/wood burning stylus, etc., she found this for
me. It is made on a sheet of 3/16" thick x ~17" high x ~24" wide plywood. I would certainly have been driven crazy (crazier?) trying to make something
similar on my scroll saw. Now I just have to make a suitable frame for it...
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[Edited on 11-13-2016 by CharlieA]
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mayko
International Hazard
Posts: 1218
Registered: 17-1-2013
Location: Carrboro, NC
Member Is Offline
Mood: anomalous (Euclid class)
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Potassium chloride (-> chlorate)
methylene chloride (general solvent)
calcium metal (-> calcium silicide)
an assortment of LEDs (nanoprisms)
al-khemie is not a terrorist organization
"Chemicals, chemicals... I need chemicals!" - George Hayduke
"Wubbalubba dub-dub!" - Rick Sanchez
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NeonPulse
Hazard to Others
Posts: 417
Registered: 29-6-2013
Location: The other end of the internet.
Member Is Offline
Mood: Isolated from Reality! For Real this time....
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my last chemical order was simply 1l methanol, 500g Copper sulfate, 750mls IPA and 100 99.9% tin granules.
We really need a thread on latest glass/equipment obtained also i think. several other users here have posted things of that nature and i have too.
I recently got a bunch of glass on the extreme cheap including:
The best item was an Isolab 2000ml sep funnel on a rectangular stand with the bosshead/ring= i checked the price and just the glass was 175$ new not
inc the stand. score!
3X 125ml sep funnels
a 250ml sep funnel
2X 500ml volumetric flasks
2X 1000ml volumetric flasks
500ml ground glass erlenmeyer 24/29
250ml wide mouth reagent jar all boro glass.
400ml Ilmabor beaker
13 medium sized test tubes plus the rack
10 small glass vials
bunsen burner+ tripod and gauze matt
quality safety goggles
3 bossheads
small bosshead/ring
3 cork lined clamps
beaker tongs, test tube tongs
some isolab pipettes 5ml and pipette bulb which looks new
electric heating matt
other bits and pieces like syringes ,disposable pipettes plastic bottles with droppers,spatulas, hose for gas bottle for the bunsen burner.
All of this cost me only $100! i could not believe my luck. i could not pass it up. The 2000ml sep funnel is worth more than that alone and the small
sep funnels were all brand new and still had the little bits of paper
in the tap to stop them getting stuck. the bunsen burner looks new as well. the tripod is still shiny and the gauze is not burnt.
[Edited on 10-12-2016 by NeonPulse]
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j_sum1
Administrator
Posts: 6219
Registered: 4-10-2014
Location: Unmoved
Member Is Offline
Mood: Organised
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woot. what a great purchase. have some fun with it.
And I agree. A proud new glassware thread is overdue. Ideally with prunings from this thread but I know that is a pretty big ask.
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Db33
Hazard to Others
Posts: 206
Registered: 25-11-2016
Member Is Offline
Mood: No Mood
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4-piperidone
heating mantle/stirrer
hotplate/stirrer
1000ml sep funnel
250ml sep funnel
2 buchner funnels, 1 sintered, 1 with holes
some filter erlenmeyers
3 neck 1000ml, 500ml round bottoms
pressurized addition funnel
vacuum pump
THAT was a good day!
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JJay
International Hazard
Posts: 3440
Registered: 15-10-2015
Member Is Offline
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Hello, everyone. It's been quite a while. I am back in civilization. Right now, I don't have a good place to do any chemistry that is smelly or
dangerous, but I'm pleased to report that my chemicals and equipment seem to have survived without a mishap!
I recently obtained several accessories for my 3000 mL 24/29 3-neck flask: a 3000 mL heating mantle, a 24/40 60 cm Dimroth condenser, a 24/40 1000 mL
addition funnel (with PTFE stopcock), and an overhead stirrer. The stirrer needs some repairs (in particular, the chuck is crooked), and I need to
build or purchase a power supply for the heating mantle, but I'm going to have a pretty sweet reaction apparatus.
Chemicals:
Calcium hydroxide
Sodium borohydride
Ammonium sulfate
Cobalt carbonate
(Oh and my first YouTube video should go up this afternoon if I can figure out how to fix a video resizing issue.)
[Edited on 11-12-2016 by JJay]
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Chlorine
Hazard to Self
Posts: 56
Registered: 26-11-2016
Location: Maine, USA
Member Is Offline
Mood: Brominated
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Two separate 25' magnesium ribbons, Potassium nitrate, sodium metabisulfate and some scrap aluminium.
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PirateDocBrown
National Hazard
Posts: 570
Registered: 27-11-2016
Location: Minnesota
Member Is Offline
Mood: No Mood
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Hmm, let's see,
From my local pottery supply:
BaCO3, 1 lb
CaCO3, 1 lb
CaF2, 1 lb
CaHPO4, 5 lb
FeSO4, 1 lb
K2CO3, 5 lb
H3BO3, 1 lb
MnO2, 1 lb
Fe2O3, 1lb
From Duda:
Glacial Acetic, 1 L
Formic, 1 L
Sulfuric, 1 L
Phosphoric, 1 L
BHT, 1 oz
Citric Acid, 5 lb
Ascorbic Acid, 1 oz
NaNO2, 1 lb
NaNO3, 1 lb
KOH, 2 lb
Ethanol, 100% 1 L
Isopropanol, 100% 1 L
Pyro Chem Source for:
K2Cr2O7 1 lb
Sr(NO3)2 1 lb
powdered carbon, 1 lb
The local brewery supply had
K2S2O5, 1 lb
I'm also fortunate to have Elemental Scientific about 6 miles from my front door.
[Edited on 12/17/16 by PirateDocBrown]
[Edited on 12/17/16 by PirateDocBrown]
[Edited on 12/17/16 by PirateDocBrown]
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j_sum1
Administrator
Posts: 6219
Registered: 4-10-2014
Location: Unmoved
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What are you going to do with more than 2kg of citric acid?
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PirateDocBrown
National Hazard
Posts: 570
Registered: 27-11-2016
Location: Minnesota
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Bath bombs!
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JJay
International Hazard
Posts: 3440
Registered: 15-10-2015
Member Is Offline
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Acetaminophen, for making hydroquinone. Every synthesis I see requires making benzoquinone first and then reducing it with iron or other mild reducing
agents. Benzoquinone seems to be a hot commodity, requiring DEA paperwork from many vendors, even though it is not specifically a listed substance
AFAIK.
I have little interest in benzoquinone at the present time, but I do want some hydroquinone.
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