Difference between revisions of "Boiling chip"
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==DIY boiling chips== | ==DIY boiling chips== | ||
| − | The easiest and cheapest way to make boiling chips is to smash porcelain or similar ceramic materials into small bits. Avoid using glazed ceramic, as it doesn't have rough surface necessary for nucleation. Broken | + | The easiest and cheapest way to make boiling chips is to smash porcelain or similar ceramic materials into small bits. Avoid using glazed ceramic, as it doesn't have rough surface necessary for nucleation. Broken pieces of sintered glass frit, as used in filtration, can also be used as boiling stones, though best to avoid using them in strongly alkaline solutions, as they will dissolve. |
Glass shards or quartz pieces can be used, but because the surface of these materials is smooth and not rough, they are not suitable. To make their surface rough, there are two ways: sandpaper the glass/quartz surface using a very abrasive material ([[Silicon carbide|SiC]], [[Tungsten carbide|WC]], diamond, etc.) to make it rough, or chemical treatment using [[hydrofluoric acid]] or hot aq. alkali ([[sodium hydroxide]], [[potassium hydroxide]]). | Glass shards or quartz pieces can be used, but because the surface of these materials is smooth and not rough, they are not suitable. To make their surface rough, there are two ways: sandpaper the glass/quartz surface using a very abrasive material ([[Silicon carbide|SiC]], [[Tungsten carbide|WC]], diamond, etc.) to make it rough, or chemical treatment using [[hydrofluoric acid]] or hot aq. alkali ([[sodium hydroxide]], [[potassium hydroxide]]). | ||
Latest revision as of 21:15, 15 August 2020
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A boiling chip, also known as boiling stone, or anti-bumping granule is an unevenly shaped rough granular material added to liquids to make them boil more calmly.
Contents
Function
Boiling chips are frequently employed in distillation and heating. When a liquid becomes superheated, a particle of dust or a stirring rod can cause flash boiling. This very rapid boiling can be extremely violent and cause reagents to splatter, possibly causing severe burns, ruining experiments, and damaging equipment. Boiling chips work by providing nucleation sites so the liquid boils smoothly without becoming superheated or bumping.
Properties
Boiling chips are made of a chemically inert material, like glass, quartz, or calcinated porcelain. They appear like flakes or beads, with a rough surface, necessary for nucleation.
Availability
Boiling chips can be purchased from lab suppliers. They are available as either glass or ceramic.
DIY boiling chips
The easiest and cheapest way to make boiling chips is to smash porcelain or similar ceramic materials into small bits. Avoid using glazed ceramic, as it doesn't have rough surface necessary for nucleation. Broken pieces of sintered glass frit, as used in filtration, can also be used as boiling stones, though best to avoid using them in strongly alkaline solutions, as they will dissolve.
Glass shards or quartz pieces can be used, but because the surface of these materials is smooth and not rough, they are not suitable. To make their surface rough, there are two ways: sandpaper the glass/quartz surface using a very abrasive material (SiC, WC, diamond, etc.) to make it rough, or chemical treatment using hydrofluoric acid or hot aq. alkali (sodium hydroxide, potassium hydroxide).
Silica gel can also be used as boiling stones, though it may burst at high temperatures.
Chemically cleaned sand can also be used when distilling liquids that tend to bump violently such as sulfuric acid.
Projects
- Anti-bumping material during distillation
- Abrasive
Safety
Boiling stones help reducing bumping during boiling, but do not eliminate it.
