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ETN recrystalization issues
Well, I repeated the synthesis this time with only 6g erythritol and without NH3, everything went fi ...
22-6-2015 at 05:10
by: Icefall
ETN recrystalization issues
Sorry for opening such an old topic; but I seem to have the very same issue as Turner had and I can' ...
4-6-2015 at 14:38
by: Icefall
Picric acid from phenol - need help
Hello again,
I've made some tests and I´d like to share them :)

Picric acid is quite difficult ...
20-2-2015 at 08:36
by: Icefall
Success!
Hello again,

The synthesis was pretty good now :cool: This time, I added phenol-sulphonic acid to ...
11-1-2015 at 09:47
by: Icefall
Picric acid from phenol - need help
Thanks for replies, the pictures look pretty good.

I think the problem was either with temperatur ...
9-1-2015 at 09:11
by: Icefall
Thx
So, according to stoichiometry, one needs 3mol of HNO3 for every 1mol of phenol. 25grams equals 0,26 ...
8-1-2015 at 22:48
by: Icefall
Picric acid from phenol - need help
Yes, I have read the first 7-8 pages of that article, I know a lot about Rosco's findings about solu ...
8-1-2015 at 13:37
by: Icefall
Picric acid from phenol - need help
Hello everybody,

I am new to this forum but I have been reading and using information from it for ...
8-1-2015 at 11:59
by: Icefall

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