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chloromethylene dibenzoate: stable formyl chloride equivalent
Can't edit the last post anymore but the thesis above:
https://aura.american.edu/articles/thesis/Sy ... |
17-3-2024 at 07:36
by: clearly_not_atara |
Separating chloroacetic acid and an sulfuric acid
Depending on how much sulfuric acid you used, it might be possible to absorb it onto anhydrous sodiu ... |
16-3-2024 at 20:39
by: clearly_not_atara |
chloromethylene dibenzoate: stable formyl chloride equivalent
^Thanks. The book is similarly circumspect. It also cites Descudé, but a different paper ([i]Compt. ... |
15-3-2024 at 21:45
by: clearly_not_atara |
Thioacetamide synthesis
Acetone is probably fine. Some amount of condensation is probably possible. But it shouldn't affect ... |
15-3-2024 at 11:15
by: clearly_not_atara |
Ethylchloride preparation
According to Raoult's law, the product is most likely a gas, since the rxn is sluggish at low temper ... |
15-3-2024 at 10:50
by: clearly_not_atara |
Thioacetamide synthesis
Do not use ethanol to recrystallize.
[quote]when hydrogen ions exists, it can generate thiosulfate ... |
15-3-2024 at 09:07
by: clearly_not_atara |
chloromethylene dibenzoate: stable formyl chloride equivalent
Wenzel in 1914 (attached) reported the reaction of chlorine with methylene dibenzoate, giving the ti ... |
14-3-2024 at 17:08
by: clearly_not_atara |
Calcium Silicate from concrete rubble?
[rquote=691536&tid=160214&author=nikotyna1939]I don't just buy calcium silicate because in m ... |
14-3-2024 at 07:47
by: clearly_not_atara |
Hydrazinol (N-amino hydroxylamine)
This is postulated as an intermediate in some oxidations of hydrazine. It is probably extremely unst ... |
13-3-2024 at 07:52
by: clearly_not_atara |
burnt through steel crucible?
Zinc seems like a likely culprit. Often alloyed with copper and tin, low bp, potentially flammable v ... |
13-3-2024 at 07:33
by: clearly_not_atara |
Synthesis of fatty acids from expired soap
Soap doesn't really expire. They just want you to buy more. Granted there will be some rancidity, bu ... |
13-3-2024 at 05:08
by: clearly_not_atara |
Calcium Silicate from concrete rubble?
You can just buy wollastonite IIRC |
12-3-2024 at 18:39
by: clearly_not_atara |
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
I think that the solubility of HCl in BzCl is probably quite low. HCl is highly volatile and only di ... |
11-3-2024 at 20:07
by: clearly_not_atara |
Failed attempts at oxidation of alcohols with DMSO/P2O5
The Swern conditions are known to attack phenols as well:
https://cir.nii.ac.jp/crid/13902826791139 ... |
9-3-2024 at 07:15
by: clearly_not_atara |
Failed attempts at oxidation of alcohols with DMSO/P2O5
Have you tried any other substrates? It's plausible that cinnamyl alcohol just acts weird here. Not ... |
8-3-2024 at 14:04
by: clearly_not_atara |
Thioacetamide synthesis
Even among thioamide preparations, this one sounds particularly dangerous. H2S at high pressure? Org ... |
8-3-2024 at 07:14
by: clearly_not_atara |
The Short Questions Thread (4)
I didn't know Yakov Smirnov posted here |
6-3-2024 at 21:51
by: clearly_not_atara |
Metallic soaps
If it forms an acetate, it should probably form a stearate. The reactivity of the carboxylate doesn' ... |
5-3-2024 at 15:17
by: clearly_not_atara |
Unexpected product in mucic acid dry distillation
Recently my thoughts came back to this.
https://www.mdpi.com/2073-4344/13/7/1114
In the above ... |
5-3-2024 at 11:14
by: clearly_not_atara |
The Short Questions Thread (4)
CAS 56138-70-6:
https://www.lookchem.com/ProductWholeProperty_LCPL1207016.htm
https://academic ... |
2-3-2024 at 08:46
by: clearly_not_atara |
pKa of an aldehydic hydrogen?
Look up "acyl anion" |
2-3-2024 at 08:36
by: clearly_not_atara |
Solvents for Lithium Hydride
There are no soluble saline hydrides in any solvents. LiH is always used heterogeneous. And yeah I d ... |
29-2-2024 at 21:38
by: clearly_not_atara |
What exactly is going on in this here molecule?
It also appears that perchloryl amides were investigated by the US military:
https://apps.dtic.mi ... |
29-2-2024 at 11:11
by: clearly_not_atara |
What exactly is going on in this here molecule?
There's a negative charge on the oxygens, a positive charge on the hydrogens, and the separation is ... |
28-2-2024 at 14:53
by: clearly_not_atara |
Pyrazine Synthesis?
I'm doubtful of the reaction of ammonia with chloroacetone. Aside from the noxious properties of the ... |
27-2-2024 at 09:29
by: clearly_not_atara |
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