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Diethylether (sulfuric acid saving method)
One substitute I read about somewhere (I can’t remember where) that you could also use is anhydrou ...
15-5-2024 at 11:59
by: Sir_Gawain
H2O2 from urea peroxide
You could also extract the hydrogen peroxide from solution with diethyl ether, but this is practical ...
13-5-2024 at 10:08
by: Sir_Gawain
Cody's lab: 50lbs Al cans to thermite: pool of liquid Al2O3
Cool video. It’s really interesting how the particle size scales up. There’s probably no limit t ...
13-5-2024 at 10:01
by: Sir_Gawain
Simple way to differentiate MEK and THF
If your solution was alkaline there wouldn’t be any bisulfite, just sulfite.
13-5-2024 at 09:51
by: Sir_Gawain
Unknown impurity in ethyl acetate
I feel really stupid; I just figured it out. I checked the density, aannndddd it's ethyl acetate. I ...
10-5-2024 at 17:14
by: Sir_Gawain
Unknown impurity in ethyl acetate
I recently bought a liter of "MEK substitute" from the hardware store. The MSDS says 100% ethyl acet ...
10-5-2024 at 16:58
by: Sir_Gawain
Nitric acid bottles growing exterior crystals?
That’s definitely the problem. You need to get a cap made out of something else—preferably Teflo ...
6-5-2024 at 22:09
by: Sir_Gawain
Simple way to differentiate MEK and THF
It should say on the can what solvents it contains. I’ve most commonly seen a mixture of MEK and T ...
6-5-2024 at 14:10
by: Sir_Gawain
Most Cost-Effective Explosive
[rquote=692920&tid=160313&author=underground]Now the problem with NQ is well known so deriva ...
6-5-2024 at 13:59
by: Sir_Gawain
PbSO4 to H2SO4
[rquote=692876&tid=160309&author=LookingForAnswers]Hello there. All sings on earth and heave ...
5-5-2024 at 20:52
by: Sir_Gawain
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Did you end up with a yield of NaNTz? It’s possible the reaction didn’t work and so none of the ...
5-5-2024 at 20:18
by: Sir_Gawain
Hydrazine
Yeah, with higher concentrations of hypochlorite, you just have to use the hydrochloric acid neutral ...
5-5-2024 at 20:12
by: Sir_Gawain
Most Cost-Effective Explosive
Aside from thermobarics, the cheapest explosives by weight are going to be ammonium nitrate based.
...
5-5-2024 at 20:07
by: Sir_Gawain
Nitric acid bottles growing exterior crystals?
It’s probably reacting with the metal cap. Do you know what metal it is?
How did you make your ni ...
5-5-2024 at 19:48
by: Sir_Gawain
Failed attempt at making chloroform[?]
That pleasant-smelling side product might be chlorobutanol. It forms from a reaction between chlorof ...
3-5-2024 at 13:21
by: Sir_Gawain
"Let's Distill Some H2SO4!" -Last Words
I think you can use too many boiling chips. While distilling ethylene glycol (b.p. 197 C), using mor ...
2-5-2024 at 08:44
by: Sir_Gawain
Failed attempt at making chloroform[?]
[rquote=692854&tid=160307&author=AndrewOfWallachia]
Is it perhaps possible that I can conce ...
2-5-2024 at 08:37
by: Sir_Gawain
Dichloromethane now banned from US paint strippers
Not here in the US. About six years ago though it was removed from most products. As Dr. Bob stated, ...
1-5-2024 at 22:15
by: Sir_Gawain
Pure CuCl2 from dirty HCl
Place an open container of the dirty acid and an open container of water inside a larger sealed cont ...
1-5-2024 at 07:36
by: Sir_Gawain
Dichloromethane now banned from US paint strippers
What about other products? I’ve never seen dichloromethane paint stripper in the last six years, b ...
1-5-2024 at 06:49
by: Sir_Gawain
New ETN Synthesis
No, just urea. It absorbs nitrogen oxides and residual acid.
29-4-2024 at 14:10
by: Sir_Gawain
"Let's Distill Some H2SO4!" -Last Words
Nurdrage recently released a video on this very topic. It’s very informative.
Even with the cer ...
27-4-2024 at 09:18
by: Sir_Gawain
Hydrazine
Since you used the sulfuric acid neutralization method and that small volume of liquid, it’s most ...
23-4-2024 at 12:02
by: Sir_Gawain
Hydrazine
[rquote=692663&tid=1128&author=ManyInterests]I wanted to ask this question and I should have ...
21-4-2024 at 18:54
by: Sir_Gawain
Hydrazine
[rquote=692658&tid=1128&author=Keras]I tried the hydrazine sulphate classic synthesis (the o ...
21-4-2024 at 12:12
by: Sir_Gawain
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