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Salt amoniac sublimation, best method???
If it falls it will land on the watchglass!
14-5-2021 at 10:05
by: njl
Pyridine hydrogenation - methods?
I'm interested in the electroreduction garagechemist mentioned, where can I find more info on that?
14-5-2021 at 09:10
by: njl
Salt amoniac sublimation, best method???

[quote]
NH3(g) + Cl(g)
[/quote]

Should be NH3 + HCl
14-5-2021 at 04:44
by: njl
N-acetyl MDA from helional
Consider the schmidt reaction of HN3 with carbonyls, which under some conditions yields formamides f ...
13-5-2021 at 14:17
by: njl
Survey: Reagent Wish List
What reducing agents would those be?
12-5-2021 at 15:12
by: njl
Aldehyde oxidation
The colors in the first reaction ranged from purple, light pink, brown, to gray, honey, and red-oran ...
12-5-2021 at 11:16
by: njl
Anhydrous Aluminum Chloride
[url=https://onyxmet.com/index.php?route=product/product&path=70&product_id=1949]Onyxmet[/ur ...
12-5-2021 at 10:21
by: njl
Survey: Reagent Wish List
Definitely clean and undiluted H2SO4, HNO3, anhydrous alcohols, I'm always looking for NaBH4 - best ...
12-5-2021 at 10:13
by: njl
Aldehyde oxidation
Because that's how they do it in the paper I linked.
11-5-2021 at 12:03
by: njl
Aldehyde oxidation
Proposed reaction scheme, .1 M scale:

A 250 mL beaker is charged with 14 g Ca(OCl)2. 150 mL room ...
11-5-2021 at 11:53
by: njl
wall wart as power supply for electrolysis
Actually, I think 2 amp phone chargers require feedback from the load in order to operate. You proba ...
11-5-2021 at 05:36
by: njl
Aldehyde oxidation
Luckily enough I have some Me2CO3. However, it is mixed with 1,3 dioxolane and I am not in a positio ...
11-5-2021 at 05:34
by: njl
Aldehyde oxidation
Seems like hypochlorite doesn't form stable solutions with many common solvents, so I think I'll be ...
11-5-2021 at 05:14
by: njl
wall wart as power supply for electrolysis
While this isn't good practice I have to admit I've used them before, they will work for some reacti ...
11-5-2021 at 05:04
by: njl
Aldehyde oxidation
Any tips for making concentrated Ca(OCl)2 solutions?
10-5-2021 at 16:03
by: njl
Aldehyde oxidation
I was avoiding acetone because it reacts violently with hypochlorite. I think isopropanol should hol ...
10-5-2021 at 10:56
by: njl
Aldehyde oxidation
I am going to try the reaction outlined in [url=https://sci-hub.st/https://doi.org/10.1016/S0040-403 ...
10-5-2021 at 10:12
by: njl
What is this metal?
[rquote=659559&tid=157392&author=vano][rquote=659557&tid=157392&author=njl]Make a fu ...
7-5-2021 at 06:42
by: njl
What is this metal?
Make a fusion weapon
7-5-2021 at 05:25
by: njl
Question about Ethyl Bromide
If you manage to make bromophosgene in this scenario you're either trying to make bromophosgene or s ...
5-5-2021 at 07:21
by: njl
Report on making metal sorbates
[quote]
The filtrate and wash water run through was red meaning either the cobalt sulphate was in e ...
5-5-2021 at 00:15
by: njl
The Short Questions Thread (4)
Carbon monoxide is a better reducing agent than it is an oxidizing agent, and ammonia needs to be ox ...
4-5-2021 at 16:30
by: njl
Acetic anhydride preparation
I think it works via addition of HCl to the nitrile to form an imidoyl chloride, this reacts with Ac ...
4-5-2021 at 08:23
by: njl
Acetic anhydride preparation
Well half of the acetonitrile is consumed as acetamide HCl. The advantage to this reaction isn't yie ...
4-5-2021 at 05:39
by: njl
Nomenclature of Coordinative Compounds
For some reason I always see Cp first as in (Cp)2[TiCl2]. Whether or not that's correct, I don't kno ...
4-5-2021 at 05:32
by: njl
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