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Ketalization of Phenol
Well, there must be another approach to forming that ring.

Were it a tropane ring, the way is wel ...
4-5-2021 at 16:05
by: zed
What is this metal?
Flame test.
4-5-2021 at 14:13
by: zed
Ketalization of Phenol
7-Azanorborn-2-one framework. https://pubchem.ncbi.nlm.nih.gov/compound/7-Azanorbornene
1-5-2021 at 18:03
by: zed
What makes liquor taste like rubbing alcohol?
Now, I had a buddy that used to produce water for his own drinking, that was totally delicious.

M ...
30-4-2021 at 13:40
by: zed
Ketalization of Phenol
On further thought, a Cyclohexanone could be "ketalized", in a manner analogous to that sometimes u ...
30-4-2021 at 13:13
by: zed
Pressure Vessel
Three Questions at once?

Making HI shouldn't require Red Phosphorus, and it shouldn't require pre ...
29-4-2021 at 03:36
by: zed
Recovery of styrene monomer from polystyrene
Yup! I think I might have posted a procedure...once upon a time.

[Edited on 29-4-2021 by zed]
29-4-2021 at 03:27
by: zed
Recovery of styrene monomer from polystyrene
Yields via pyrolysis are pretty good.

For some unknown reason, this video isn't starting at the b ...
28-4-2021 at 07:31
by: zed
Path to 4-Anisaldehyde
Ummm. Anethole usta be as common as dirt.

Anise, which grows wild in these parts, is saturated w ...
28-4-2021 at 05:08
by: zed
Preparation of 2-hydroxybenzylamine
I like the yield of that Na-Amalgam reduction. Straight forward method.

Form the Oxime. Reduce ...
25-4-2021 at 14:10
by: zed
Distillation Ideas
My local cafe owner usta clean out his Coffee pots with "Dutch Cleanser" and ice. Put a little clea ...
25-4-2021 at 13:33
by: zed
Pyrimethamine Synthesis?
Well, it has been a while, but I did stumble across a paper related to this topic today.

A decent ...
24-4-2021 at 18:40
by: zed
A Note on the Synthesis of 3-Nitrophthalic Acid
Seems to me, the nitration of Naphthalene, produces a glorious yield of almost entirely the right is ...
24-4-2021 at 05:58
by: zed
Dichromate overoxidation
Bovinejony... Indoles are a horse of different color.

They don't take kindly to being oxidized, ...
24-4-2021 at 02:07
by: zed
Methyl iodide (iodomethane) woes (Red P method)
Red phosphorus is hard to come by in the USA. I don't know where you are, but you might find it dif ...
24-4-2021 at 01:45
by: zed
Preparation of 2-hydroxybenzylamine
Well, it seems like there might be difficulties. I expect aromatics to behave like aromatics. Pret ...
24-4-2021 at 00:53
by: zed
Preparation of 2-hydroxybenzylamine
Ummm. Salicyl Alcohol + HCl ---> Salicyl Chloride

Salicyl Chloride + NH3 (or Potassium Phthla ...
23-4-2021 at 23:46
by: zed
Ketalization of Phenol
Back to Phenol. Phenol is already in "its Enol form", if you were to consider phenol to be a waywar ...
22-4-2021 at 09:16
by: zed
What is happening at Deschem?
Well, rather than speculating..... I sent Deschem a message via Ebay.

They got back to me right ...
22-4-2021 at 08:48
by: zed
Ketalization of Phenol
You are kinda leaving us without background.

Looks like you are exploring the synthesis of some u ...
21-4-2021 at 22:21
by: zed
Anisoin
Your initial link. My Mac can't open it. Gotta PDF?

21-4-2021 at 21:52
by: zed
Trying to get potassium permanganate out of solution, keeps turning to MnO2
Which is exactly why I figure to buy mine in a bottle. Trying to make it, messes with my absolutist ...
21-4-2021 at 07:47
by: zed
Ketalization of Phenol
Haven't really thought of it.

Phloroglucinol can behave like a Ketone.

It can actually be conv ...
21-4-2021 at 01:18
by: zed
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
It should be noted, that the Jademyr paper, proceeds to the synthesis of NBOME analogs. A perilous ...
20-4-2021 at 12:10
by: zed
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
Umm. Once upon a time... I conducted plenty of attempts at reducing Nitro-Olefins via NaBH4-Boride ...
20-4-2021 at 10:36
by: zed
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