I don't get it, why wouldn't you use an azeotrope of acetic acid instead? That way instead of having to boil off 97% of the solution you only have to
boil off 3%. As an example, wikipedia lists an azeotrope of acetic acid/n-heptane that boils at 92.3°, and is 70% acetic acid. Admittedly 92.3° is a
bit too close to the boiling point of water for comfort but that was just an example, I'm sure there are others. |