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Author: Subject: Nickel benzoate
vano
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[*] posted on 21-12-2020 at 11:42
Nickel benzoate


What do you think? Has anyone tried this?


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njl
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[*] posted on 21-12-2020 at 12:23


Source?
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RustyShackleford
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[*] posted on 21-12-2020 at 12:32


I have tried thermal decomposition of calcium benzoate to make benzophenone but it didnt work at all
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[*] posted on 21-12-2020 at 12:35


Quote: Originally posted by njl  
Source?


Chinese wikipedia.
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valeg96
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[*] posted on 21-12-2020 at 22:41


My best guess is that those claims come from some negligible literature results, at least on the productive scale. Whoever reported that probably ran the combustion or TGA fumes through a GC-MS and identified all those molecules in traces.

Sure, if you heat to decomposition Ni benzoate you probably can find a couple ppm of biphenyl in the fumes, but that's miles away from being a productive route. If it was that simple, biphenyl wouldn't be that expensive, for one thing.





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JJay
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[*] posted on 22-12-2020 at 13:01


Quote: Originally posted by RustyShackleford  
I have tried thermal decomposition of calcium benzoate to make benzophenone but it didnt work at all


Did you use a vacuum? I'm pretty sure that's a viable synthetic method (though undoubtedly low-yielding).
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