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Drying heating oil
Okay, here we enjoy a practical application of chemistry.

I want to remove the water, if any, fro ...
25-9-2015 at 12:34
by: CaptainPike
Preparation of Salicylaldehyde
Magpie,

We love you – you make the absolute best OC Porn, ever!
4-9-2015 at 16:52
by: CaptainPike
Trouble Cleaning DCM
+Mr.HomeScientist – good idea. I looked up the word, "entrainment", Dictionary.com says
[i]
to ...
25-6-2015 at 17:38
by: CaptainPike
Trouble Cleaning DCM
I bought a can of dichloromethane on eBay, a half-gallon, or something – in a metal can just like ...
25-6-2015 at 11:04
by: CaptainPike
Bad Habits In The Lab
I sometimes squirt the pipette of pure acid back in the mother container – which can contaminate. ...
3-5-2015 at 16:14
by: CaptainPike
Best non-polar solvent for caffeine
Check out the YouTube [url]https://www.youtube.com/watch?v=Xzh-6ZDitQ8 [/url] video where Dr Rob St ...
3-2-2015 at 08:15
by: CaptainPike
Benzyl Alcohol Extraction
the standard is 29/42. The overseas guys produce a lot of joints that are 29/(some number less than ...
2-2-2015 at 09:07
by: CaptainPike
Acetic Acid Synth. Easy Home Version.
That wasn't too bad a, "Whack", after all!

Thank you, S.C., for the following procedure, which ma ...
15-1-2015 at 12:05
by: CaptainPike
Acetic Acid Synth. Easy Home Version.
[rquote=368432&tid=29728&author=Dronami_inc]elegant solution :)
If I understand properly, ...
13-1-2015 at 17:08
by: CaptainPike
Synthesis of Benzocaine
… but seriously folks

No actual coke dealer would cut his product with benzocaine. Especially i ...
12-1-2015 at 04:49
by: CaptainPike
Acetic Acid Synth. Easy Home Version.
Yes, I started a new thread.

Maybe as you imply, it should be just a post in the thread that I in ...
11-1-2015 at 13:04
by: CaptainPike
GAA/ethanol prep – Harmless Home Lab Version

[b] Background [/b]
A one mole scale experiment was performed along the lines of a procedure post ...
11-1-2015 at 12:41
by: CaptainPike
OTC Calcium Chloride - Good for Drying
I have baked the cheap stuff that comes in the huge bag from Walmart (or at every convenience store, ...
6-1-2015 at 14:00
by: CaptainPike
Acetic Acid Synth. Easy Home Version.
Does anybody believe this reaction can occur (and go to completion) in a reaction media of ethyl ace ...
31-12-2014 at 19:14
by: CaptainPike
Acetic Acid Synth. Easy Home Version.
[b] THERE! I have officially gotten tomatoes thrown at me [/b]

Are you talking to me?
26-12-2014 at 13:31
by: CaptainPike
Neat and Cheap – EtOH, GAA!?
Okay, I'll probably appear to be cocky,this is not my intent, but could this thing be as perfect as ...
25-12-2014 at 21:21
by: CaptainPike
First Major Lab Accident
Wow, thank God (or good old numerical probabilistic outcome) you were working in a fume hood. Thank ...
24-12-2014 at 12:41
by: CaptainPike
Simple Argon Source
TY Bob – this is just the ticket for small scale stuff and backfilling reagent bottles. I wrote to ...
3-12-2014 at 15:35
by: CaptainPike
Clean Ethanol from OTC Yeasts and chemicals
DAMN, I wish I had found this thread earlier.

About when you started (back in September) I was ho ...
2-12-2014 at 18:25
by: CaptainPike
a neglected halo–form
… and another thing! (Pardon my shameless re-fibrillation of this thread)

Looking at this pictu ...
25-11-2014 at 18:11
by: CaptainPike
a neglected halo–form
some more images.
These photos show the addition of a few more milliliters of acetone to an already ...
10-11-2014 at 19:55
by: CaptainPike
a neglected halo–form
I needed some chloroform, and repeated a procedure I have used several times. This procedure was pre ...
3-11-2014 at 11:08
by: CaptainPike
Recrystallizing Zinc Chloride
Thank you, Dots for your educative response. I have little doubt that the pathway you have outlined, ...
1-11-2014 at 09:34
by: CaptainPike
Recrystallizing Zinc Chloride
I got a great deal on some zinc chloride from overseas. I waited quite a while for it and I was exci ...
26-10-2014 at 09:44
by: CaptainPike
Synthesis of Benzocaine
This is a very popular prep on YouTube. I guess there may be some recreational usage avenues there s ...
26-10-2014 at 08:50
by: CaptainPike
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