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Preparation of elemental phosphorus
While buying some steel pipe to build an apparatus to try this with trisodium phosphate, I found a l ... |
11-6-2016 at 12:05
by: DFliyerz |
Broken Vigreux Column
A while ago I got a 100mm Vigreux column but very clumsily broke it soon after getting it. I kept it ... |
3-6-2016 at 20:39
by: DFliyerz |
Collecting solid from filter paper after filtration - what is the proper technique?
This is a completely wild guess, but are the high value solids gold or PGMs that are to be re-dissol ... |
3-6-2016 at 11:02
by: DFliyerz |
Preparation of Neodymium Sulfate from Magnets
Beautiful crystals! I'm glad that someone finally posted a procedure, seeing as the other really goo ... |
2-6-2016 at 10:11
by: DFliyerz |
Sucrose -> THF
I'm trying to figure out a decent way to make 1,2-dichloroethane from ethylene glycol, preferably us ... |
27-5-2016 at 07:56
by: DFliyerz |
Sucrose -> THF
Two more documents describing conversion of cellulose, sucrose, and other similar carbohydrates to c ... |
26-5-2016 at 10:18
by: DFliyerz |
Sucrose -> THF
There are some other methods of synthesizing chloromethylfurfural, which have recorded yields of up ... |
26-5-2016 at 10:03
by: DFliyerz |
Sucrose -> THF
I was wondering what the viability of a synthesis of furan and tetrahydrofuran from sucrose was. My ... |
26-5-2016 at 07:42
by: DFliyerz |
Al/NiCl2*6H2O: OTC hydride-like reactivity
Definitely looks good! When I have time I'll try it with methanol and nitrobenzene. |
25-5-2016 at 10:19
by: DFliyerz |
Tube Furnace Reactions
Additionally, for reactions between two gasses, how do you keep the flow rates to the correct propor ... |
13-5-2016 at 15:17
by: DFliyerz |
Dried my DCM and now I have some tiny bubbles on the bottom, are these peroxides?
Personally, I think that the best stabilizer choices for DCM are ethanol, methanol, and (if you can ... |
13-5-2016 at 11:42
by: DFliyerz |
Possible route to Toluene from Xylene
In many places, people can get mixed xylenes easily but can't get toluene. While looking around, I f ... |
13-5-2016 at 07:05
by: DFliyerz |
Tube Furnace Reactions
I recently acquired a tube furnace from someone here as well as 8' of quartz tubing from eBay. I was ... |
12-5-2016 at 08:31
by: DFliyerz |
Cheap glassware
Despite the stigma of Chinese suppliers on eBay having poor quality glassware, I've had only good ex ... |
12-5-2016 at 08:07
by: DFliyerz |
Shedworld Reloaded
So, so jealous! It's like watching porn for a chemist. But now I know what I want my work space to l ... |
12-5-2016 at 07:38
by: DFliyerz |
DIY/Cheap Tube Reactor
Another reaction that would be a primary use for a tube furnace for me would probably be making alum ... |
15-4-2016 at 09:10
by: DFliyerz |
DIY/Cheap Tube Reactor
Hmm, interesting! One of the reactions that I was considering looking into was a low-pressure conver ... |
14-4-2016 at 20:45
by: DFliyerz |
DIY/Cheap Tube Reactor
Can any of these designs be used for reduction of oxides? How would the powders be loaded? |
14-4-2016 at 18:11
by: DFliyerz |
DIY/Cheap Tube Reactor
Does anyone have a design or a source for a relatively inexpensive tube reactor? I may not be using ... |
14-4-2016 at 10:27
by: DFliyerz |
Potassium Iodide
[rquote=445088&tid=65899&author=JJay]Those aren't exactly screaming deals on potassium iodid ... |
11-4-2016 at 20:54
by: DFliyerz |
Potassium Iodide
While looking for a source of iodine, I found Purebulk selling pure potassium iodide: http://purebul ... |
11-4-2016 at 09:52
by: DFliyerz |
Aniline
Here's some stuff on aniline via benzamide:
http://www.sciencemadness.org/talk/viewthread.php?tid=4 ... |
7-4-2016 at 11:53
by: DFliyerz |
Best way of converting salts to Ni(NO3)2and Co(NO3)2
Carbonate is generally a good choice, since it precipitates reliably without any complex forming and ... |
26-3-2016 at 12:36
by: DFliyerz |
Disproportionation of phenylphosphinic acid: OTC triphenylphosphine?
I'm a little confused: how is phenylphosphinic acid OTC? |
19-3-2016 at 14:57
by: DFliyerz |
Toluene in Washington
[rquote=439719&tid=65385&author=elementcollector1]Having lived in western WA, I can safely s ... |
25-2-2016 at 18:58
by: DFliyerz |
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