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Capsazepine Synthesis
OK, as a small incentive*, I'll offer ~2.5 g or so of fairly pure brominated cinnamic acid (synthesi ...
14-5-2017 at 03:34
by: Eddygp
Capsazepine Synthesis
I doubt you would lose methoxy like that in the 7-m. cyclisation step. Maybe a sulfonate ester would ...
8-5-2017 at 01:12
by: Eddygp
The Short Questions Thread (4)
Is there any simple way to dehydrate ketones to the corresponding alkyne?
4-4-2017 at 01:56
by: Eddygp
Synthesis of tetrahydrofuran derivative?
True, conjugate addition is a fairly good competing reaction.
Nevertheless, will the following cycl ...
17-3-2017 at 07:09
by: Eddygp
Synthesis of tetrahydrofuran derivative?
I was messing around for a while and thought about a possible synthesis (attachment). It seems fairl ...
15-3-2017 at 08:22
by: Eddygp
Making bromine (super cheap and easy, no destillation, quantitative yield)
Nitrosyl bromide itself would be interesting as a reagent to be fair.
8-3-2017 at 13:13
by: Eddygp
Small scale dehydrogenation
It probably depends a lot on what system you are trying to dehydrogenate. There were these articles. ...
6-3-2017 at 13:11
by: Eddygp
Unique silver compounds
[rquote=474234&tid=72224&author=DraconicAcid]The black solid formed by the reaction with asc ...
10-2-2017 at 08:22
by: Eddygp
Benzaldehyde synthesis using aqueous nitric acid
Ogata Y, Sawaki Y, Matsunaga F, Tezuka H. Kinetics of the nitric acid oxidation of benzyl alcohols t ...
9-2-2017 at 05:45
by: Eddygp
Mixed Salt System Solubility
I'm pretty sure there will be no barium sulphate.

Either way this is just a bit of spoonfeeding - ...
6-2-2017 at 07:50
by: Eddygp
On the synthesis of nanocrystals
I have always found nanocrystals fascinating, they tend to have very interesting optical behaviours ...
28-1-2017 at 11:43
by: Eddygp
Transform manganese oxide (III) into manganese oxide (IV)
Fortuately Mn(n+) will be easy to reduce with many things. C is possible, manganese carbide could be ...
28-1-2017 at 11:14
by: Eddygp
Reaction of pyridine with [Cu(Cl)2(H2O)2] product is pyridine complex or the hydroxide ?
[rquote=472605&tid=71898&author=DraconicAcid]I stand corrected.

However, just because you ...
23-1-2017 at 10:01
by: Eddygp
When drying salts how do you prevent cake formation sticking to glass?
There are a few impermeability/anti-stick spray on products around. You could potentially use that o ...
11-1-2017 at 07:08
by: Eddygp
Potassium Perchlorate from Potassium Chlorate
Xenon trioxide
10-1-2017 at 03:03
by: Eddygp
Cleaning Denatured Ethanol
DMSO was banned because of improper use, i.e. people indiscriminately using huge quantities of it as ...
9-1-2017 at 12:48
by: Eddygp
Ligands derived from niacin?
(possibly N-substituted) nicotinamide? More stable and much less reactive than acids or esters under ...
9-1-2017 at 07:18
by: Eddygp
Nitrogen adds to Double Bond
[rquote=471109&tid=71658&author=Crowfjord]It's definitely a 1,4 addition and it works due to ...
7-1-2017 at 07:02
by: Eddygp
How stable is TEMPO to heat?
There is a flash point recorded in SigmaAldrich MSDS at 67ÂșC so probably fine - maybe a very small ...
4-1-2017 at 08:41
by: Eddygp
Preparation of phosphorus halides from phosphorus pentoxide
P=O bonds tend to be very strong, which makes many reactions, like the Wittig reaction, thermodynami ...
30-12-2016 at 07:23
by: Eddygp
Sodium Carbonate and Aluminum reaction
The above equation is neither balanced, nor does the "trialuminium dihydroxide" exist... you magical ...
30-12-2016 at 07:14
by: Eddygp
Tantalum Recovery Experiment from Tantalum Capacitors
Could you please post some text, information, discussion when posting your videos? Because otherwise ...
30-12-2016 at 07:11
by: Eddygp
Synthesis of t-nitrosobutane (w/ pictures)
Very nice, numos!! Always nice to read about some more chemistry - I also kind of like nitroso compo ...
30-12-2016 at 07:06
by: Eddygp
Plant Material Extraction
I'd never even heard of Celite either ! So much to lea ...
25-12-2016 at 04:19
by: Eddygp
Potassium nitrite solution
If it's wet, it will be very difficult to determine the exact concentration without a margin of erro ...
16-12-2016 at 05:36
by: Eddygp
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