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Does anyone have experience using TBAB as a PTC? Does it cause emulsions? I was planning to run the reaction from the start with only separable solvents, such as Xylene/Water ... |
28-12-2016 at 08:21 by: FireLion3 |
Does anyone have experience using TBAB as a PTC? Does it cause emulsions? I've been thinking of playing around with some phase transfer catalyst reactions and got my hands on ... |
27-12-2016 at 22:18 by: FireLion3 |
Can I separate amines of different polarity/bulkiness via partial A/B extraction? I'm not talking about separating them based on differences in acidity, but rather sterics or hydroph ... |
6-9-2016 at 08:59 by: FireLion3 |
Can I separate amines of different polarity/bulkiness via partial A/B extraction? Couldn't find any information on this but it seems like it would work in theory.
If there is a 5 ... |
6-9-2016 at 07:49 by: FireLion3 |
Caustic Vapor from adding Sodium Hydroxide to water? But this all still begs the question, how is an aerosol getting created? I've had these caustic vapo ... |
13-4-2016 at 21:57 by: FireLion3 |
Caustic Vapor from adding Sodium Hydroxide to water? I didn't realize something such as Sodium Hydroxide could be so easily volatile into the air, especi ... |
11-4-2016 at 12:05 by: FireLion3 |
Caustic Vapor from adding Sodium Hydroxide to water? This has stumped me for years now and I've never really been bothered enough to look into it until n ... |
11-4-2016 at 11:39 by: FireLion3 |
What's the best way to recover Pd from Pd-Organic complexes? I'll try heating it, though I don't think I have an inert atmosphere at my disposal, but metal salts ... |
1-3-2016 at 18:04 by: FireLion3 |
What's the best way to recover Pd from Pd-Organic complexes? I have a bunch of Pd that is bound to some organic (phosphine) complexes (in the form of PdCl2), and ... |
1-3-2016 at 17:36 by: FireLion3 |
Does DMSO dissolve..... glass, to any extent? Hm. I did remove one of the stoppers briefly and it still appears to be unfrosted, but then again I ... |
4-2-2016 at 20:23 by: FireLion3 |
Does DMSO dissolve..... glass, to any extent? I feel like this is a dumb question but I have to ask.
For the first time ever I was using DMSO ... |
4-2-2016 at 20:08 by: FireLion3 |
Boiling to dryness - risk of explosion? I should be okay then. There are no organics in the mixture, and yes the metal is Pd (as indicated b ... |
14-12-2015 at 20:35 by: FireLion3 |
Boiling to dryness - risk of explosion? Boiling some leftover aqua regia + water mixture off to recover a metal salt, and I need to boil it ... |
14-12-2015 at 19:27 by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia... @gdflp
Back suction of the neutralizing solution would introduce the carbonate resulting in sodi ... |
22-10-2015 at 16:14 by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia... I did some googling and found one source say that it's not exclusive HCl that will cause palladium t ... |
21-10-2015 at 19:25 by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia... I wasn't sure how to interpret the soluble in trace amounts note. So you think if I neutralize all t ... |
21-10-2015 at 16:06 by: FireLion3 |
Need some advice/help on recovering Palladium from Aqua Regia... What I thought would be a two day process of dissolving the Pd and boiling excess off, has become a ... |
21-10-2015 at 15:31 by: FireLion3 |
What kind of non-acidic solvent can I use for PdCl2? Does chloroform dissolve Palladium Chloride? I actually have some on hand. I googled that and couldn ... |
8-10-2015 at 16:31 by: FireLion3 |
What kind of non-acidic solvent can I use for PdCl2? I'm trying to form a PdCl2 complex and need to avoid the use of acidic solvents. I've read PdCl2 is ... |
8-10-2015 at 15:43 by: FireLion3 |
Do aryl amines react with alkyl halides? Aryl Amines have never been much interest to me, and I wasn't able to find information about this on ... |
7-9-2015 at 01:37 by: FireLion3 |
Handling Benzoyl Chloride? That's good. I have a pretty good filter system. My experience with Benzyl Chloride also had it heat ... |
13-8-2015 at 00:15 by: FireLion3 |
Handling Benzoyl Chloride? I was planning to get some of this for a Benzoylation reaction, since the Anhydride seems to be supe ... |
11-8-2015 at 22:13 by: FireLion3 |
Is Raney Nickel inherently flamable, or only after pressure reactions? [rquote=376562&tid=35812&author=CuReUS][rquote=376307&tid=35812&author=FireLion3]Guy ... |
10-12-2014 at 09:08 by: FireLion3 |
Is Raney Nickel inherently flamable, or only after pressure reactions? I'm not worried about storing it post reaction. I am more concerned with storing the unused Raney Ni ... |
9-12-2014 at 14:10 by: FireLion3 |
What is the mechanism for catalytic cleavage of ethers by Lewis Acid's? [b]forgottenpassword[/b],
If you had been paying attention to the thread you would see that such ... |
9-12-2014 at 10:53 by: FireLion3 |
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