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.1 M Water?
I am trying it your method today. Previously I just decided to throw in a 1:2 eq h2o:etoh, and the r ... |
6-5-2013 at 12:15
by: GreenD |
.1 M Water?
If only they would have thrown in "respectively" |
6-5-2013 at 10:11
by: GreenD |
Solid-Liquid Azeotropic Distillation
This paper
http://www.ncbi.nlm.nih.gov/pubmed/18498150
describes a procedure:
"The product was ... |
25-4-2013 at 14:11
by: GreenD |
.1 M Water?
Well the paper literally skims over this, as it is a "general procedure" and says
"Reagent A - 1eq ... |
24-4-2013 at 19:57
by: GreenD |
.1 M Water?
Bit confused.
Paper calls for a solution of reagents - (1eq and 1.2 eq - not that it matters) but ... |
23-4-2013 at 14:05
by: GreenD |
Physical Chemistry Software
Hey all.
I'm wondering if anyone has preferences for molecular modeling software. I have a molecule ... |
16-4-2013 at 09:34
by: GreenD |
5000mL distillation
depends... do you have 2 setups?
If you have two set ups the 2x2000mL is going to go at less than h ... |
3-4-2013 at 23:26
by: GreenD |
drying tube... odd configuration
I don't get it, whats the point of the curvature |
3-4-2013 at 23:24
by: GreenD |
drying tube... odd configuration
Hey, I've only worked with drying tubes once before and they were simple and straight like this:
... |
3-4-2013 at 09:38
by: GreenD |
Regeneration of carbodiimides
Whoa:
"Procedure for regeneration of PS-cyclohexylcarbodiimide (PSCC). The polymer bound cyclohexyl ... |
27-3-2013 at 10:59
by: GreenD |
Regeneration of carbodiimides
Hey,
I'm trying to find a good general procedure for regenerating carbodiimides from the urea pro ... |
27-3-2013 at 10:44
by: GreenD |
Odd ratio, help?
A paper is suggesting column chromatography:
"...(Silica gel, 230-400 mesh, [b]Et[sub]2[/sub]O/pent ... |
25-3-2013 at 13:45
by: GreenD |
microscale column chromatography
Preparative TLC sounds like a great option, thanks very much. |
14-3-2013 at 19:23
by: GreenD |
microscale column chromatography
[rquote=277768&tid=23681&author=kristofvagyok]The only important thing is to use really fine ... |
14-3-2013 at 10:26
by: GreenD |
microscale column chromatography
I have done on pasteur pipettes, but it was only to achieve a truly crude product.
Thanks guys. ... |
14-3-2013 at 10:24
by: GreenD |
Latest chemical order?
Benzyl Amino Purine |
13-3-2013 at 12:18
by: GreenD |
microscale column chromatography
General question, have any of you done column chromatography with small amounts of compounds - 5-20m ... |
13-3-2013 at 12:12
by: GreenD |
SOCL2 -> Acid Chloride... Overnight?
Attempted again;
5g 0-methoxybenzoic acid was added to 25mL SOCl2 and the reaction stirred and brou ... |
20-2-2013 at 10:17
by: GreenD |
Nitriles - nucleophilic or electrophilic
PRetty clear, thanks. |
15-2-2013 at 16:09
by: GreenD |
Nitriles - nucleophilic or electrophilic
A friend made the claim that the Nitrogen of a nitrile would be nucleophilic, like the oxygen of a c ... |
15-2-2013 at 15:40
by: GreenD |
SOCL2 -> Acid Chloride... Overnight?
So.. Do you have any idea what I synthesized there?
I am out of LC/MS solvent at the moment but ... |
11-2-2013 at 16:23
by: GreenD |
SOCL2 -> Acid Chloride... Overnight?
Lo Siento.
The reaction was simple;
5g of o-methoxybenzoic acid was dissolved in 50mL of Thion ... |
11-2-2013 at 10:38
by: GreenD |
SOCL2 -> Acid Chloride... Overnight?
Totally lost now.
Tried to distill off the liquid, and the current temperature reading is 110°C. ... |
10-2-2013 at 10:26
by: GreenD |
SOCL2 -> Acid Chloride... Overnight?
I had a reaction of SOCl2 in with a benzoic acid which is reported to be quantitative under reflux f ... |
10-2-2013 at 09:52
by: GreenD |
Esterification scale-up = problems?!
So letting the reaction run over night, it went to completion.
For my work up I simply cool the ... |
24-1-2013 at 10:50
by: GreenD |
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