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Acetic anhydride preparation
I thought I'd add in some interesting details of the preparation of the MsCl - not because it is off ...
13-6-2008 at 03:33
by: LSD25
Acetic anhydride preparation
I take it most people here are at least aware of the proposed or cited synthesis of AA from methanes ...
12-6-2008 at 06:46
by: LSD25
Preparation of elemental phosphorus
[quote][i]Originally posted by garage chemist[/i]
I have not done research into this, but I have he ...
10-6-2008 at 00:41
by: LSD25
Preparation of elemental phosphorus
Grab this quick before the link dies: http://www.4shared.com/get/29938851/273f5647/Topics_In_Phospho ...
9-6-2008 at 19:22
by: LSD25
Functionalization of silica gel without silanes, solid supported TEMPO catalysts?
Once again with the double, but I cannot attach two articles

Here is a review on supported reagen ...
9-6-2008 at 18:48
by: LSD25
TEMPO substitute?
Too tired to think it through at the present time, but it struck me as odd, we have an amine which f ...
9-6-2008 at 07:32
by: LSD25
TEMPO substitute?
I'll grab some benzoate salts and try the ammonium benzoate method, at least I should get something
...
9-6-2008 at 06:26
by: LSD25
Functionalization of silica gel without silanes, solid supported TEMPO catalysts?
Here is something else, PS/PMMA were copolymerised and then sulfonated with SO3(g). The authors clai ...
8-6-2008 at 22:45
by: LSD25
Functionalization of silica gel without silanes, solid supported TEMPO catalysts?
Sorry about the double-post but I wanted to attach this one (attached) where the researchers claim t ...
8-6-2008 at 19:21
by: LSD25
Functionalization of silica gel without silanes, solid supported TEMPO catalysts?
Of some small interest might be this article:

http://pubs.acs.org/cgi-bin/abstract.cgi/jcchff/200 ...
8-6-2008 at 17:06
by: LSD25
Unconventional Shaped Charges
aha, that does make it clearer - they are probably supplying the insurgents in Iraq something simila ...
6-6-2008 at 22:21
by: LSD25
Preparation of elemental phosphorus
Got a ref or at least some more information than that? Glass, metal or quartz tube? I am more than h ...
5-6-2008 at 13:29
by: LSD25
Preparation of elemental phosphorus
I have had this recurring thought and it concerns me 'cos I don't see why it wouldn't work - I thoug ...
5-6-2008 at 11:11
by: LSD25
Synthesis of 3-(p-Hydroxyphenyl)-2-Butanone "raspberry ketone"
Sorry, I posted something which Solo had already posted (thought that sucker looked familiar).

BT ...
5-6-2008 at 10:18
by: LSD25
Sodium Ethoxide and anhydrous EtOH
OK, just found this (I condensed two articles into one download), the first details the use of catio ...
2-6-2008 at 18:08
by: LSD25
stump remover
[quote][i]Originally posted by Dilligaf[/i]
In the USA Gordon Stump remover, about $8 per pound. It ...
1-6-2008 at 19:46
by: LSD25
Functionalization of silica gel without silanes, solid supported TEMPO catalysts?
Nicodem,

Is it possible to nitrate & then reduce Lignin to a primary amine resin? If so, coul ...
31-5-2008 at 22:32
by: LSD25
Unconventional Shaped Charges
The answer to why the 'supposed' Iranian designed ATGM's are so effective is spelled 'KORNET' (AT-14 ...
29-5-2008 at 17:20
by: LSD25
Ideas for making ethylenediamine?
Could you go via the glutamine route with TCCA - should give the 4-carbon should give the 4 carbon a ...
23-5-2008 at 18:06
by: LSD25
Unconventional Shaped Charges
Design, analyses & field testing information of a 0.7m shaped charge (apparently the worlds larg ...
23-5-2008 at 11:42
by: LSD25
(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid)
[quote][i]Originally posted by Jor[/i]
Just bought 100g of metaphosphoric acid, for 8 british pound ...
21-5-2008 at 23:39
by: LSD25
Ammonium Pyrosulfate
I forgot to attach the article I cited, I believe it dealt with some of the points you raised regard ...
21-5-2008 at 20:40
by: LSD25
Ammonium Pyrosulfate
I just finished reading this article (attached) and thought it might be best placed here.

Apparen ...
20-5-2008 at 22:12
by: LSD25
Solvant-free Decarboxylation of Amino-acid
Methyl.Magic,

Could you please give details of the procedure, heat source, etc. Also do you have ...
18-5-2008 at 21:23
by: LSD25
Titanium Isopropoxide Reductive Amination
I am looking seriously at how to isolate a product which appears to be semi-immune to my favourite w ...
16-5-2008 at 17:28
by: LSD25
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