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Question about amine protection for Grignard reaction
Imagine you need to form a Grignard reagent from a molecule containing both a halogen (from which we ... |
26-3-2022 at 00:27
by: Monoamine |
Question: Storing chlorine in solution
Thank you for all the advice! I also read that sulfuryl chloride can be used as a source of Cl-, as ... |
13-3-2022 at 18:26
by: Monoamine |
Question about SO2 generation
I'm currently trying to make some sulfuryl chloride (SO[sub]2[/sub]Cl[sub]2[/sub]), which can be mad ... |
12-3-2022 at 13:12
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Aaaand... were back.
Ok I did TLC with pure naphthalene and with pure nitrobenzene to see if they ... |
5-3-2022 at 22:47
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Actually, looking at these again I'm noticing that the brightest (orange) spot is actually still at ... |
5-3-2022 at 17:24
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
I used nitrobenzene as the solvent, since it is polar enough to dissolve the AlCl3 complex so the re ... |
5-3-2022 at 17:02
by: Monoamine |
Analysis
So I finally tried this experiment and got a decent looking brown oil that had a smell of orange pee ... |
5-3-2022 at 00:47
by: Monoamine |
Triethylsilane
Actually, the method from this paper is for trypropylsilane, but this should be readily adaptable to ... |
1-3-2022 at 21:16
by: Monoamine |
Yes!
I'm actually super interested in this topic!! I just ordered all the raw materials I need to synthes ... |
1-3-2022 at 21:01
by: Monoamine |
a novel phenylmorpholine synthesis aka preludin
If preludin is what you want as the end-product, then you may just want to look into obtaining a chl ... |
1-3-2022 at 20:49
by: Monoamine |
Question: Storing chlorine in solution
I'm wondering if there is a way to make a stable solution of chlorine.
For instance would chlori ... |
19-2-2022 at 09:08
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Hi Fery, thank you for the link for the reagent supplier! My mouth is watering seeing all the wonder ... |
3-2-2022 at 21:42
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Thank you for the tips!
I'm planning to use anhydrous AlCl3 as the catalyst. From what I read, th ... |
2-2-2022 at 23:05
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
I'm planning to do my first acylation experiment soon, but I've never done this reaction, so I'm a b ... |
2-2-2022 at 05:35
by: Monoamine |
Leonid Learner's Book
Hi Basement,
Props for mentioning Leonid Lerners book: "Small scale synthesis of laboratory reag ... |
29-1-2022 at 14:01
by: Monoamine |
Solvents ?
I really don't understand why people seem to use chlorinated solvents for performing AlCl[sub]3[/sub ... |
19-1-2022 at 11:32
by: Monoamine |
Question about Grignard reaction
Thank you for all of these valuable tips! Using a Toluene and THF sounds very useful. Also thank you ... |
29-12-2021 at 13:31
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669165&tid=158187&author=S.C. Wack]Add another SO2.
Also, 2SO3 + SOCl2 -> S2O5 ... |
28-12-2021 at 21:43
by: Monoamine |
Question about Grignard reaction
I'm going to try out a Grignard reaction for the first time soon and I want to make sure I get it ri ... |
28-12-2021 at 21:39
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669124&tid=158187&author=teodor]
No, probably until the excess of Br2 will be metab ... |
25-12-2021 at 03:07
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
Hi bibliomaster. Thank you for the insights. I'm starting to suspect that pyrosulfurylchloride may a ... |
25-12-2021 at 03:04
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669117&tid=158187&author=teodor]I am dreaming of getting SOBr2 from the reaction of ... |
24-12-2021 at 08:29
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668988&tid=158187&author=teodor]Monoamine,
I have enough quantity of SOCl2 and th ... |
24-12-2021 at 03:48
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669033&tid=158187&author=Bedlasky]Very impressive work Monoamine! I really enjoyed r ... |
24-12-2021 at 03:37
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669078&tid=158187&author=Alucard]
It's very strange cause Na2S2O7 melts about 400 ... |
23-12-2021 at 13:31
by: Monoamine |
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