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Question about Grignard reaction
I'm going to try out a Grignard reaction for the first time soon and I want to make sure I get it ri ...
28-12-2021 at 21:39
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669124&tid=158187&author=teodor]
No, probably until the excess of Br2 will be metab ...
25-12-2021 at 03:07
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
Hi bibliomaster. Thank you for the insights. I'm starting to suspect that pyrosulfurylchloride may a ...
25-12-2021 at 03:04
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669117&tid=158187&author=teodor]I am dreaming of getting SOBr2 from the reaction of ...
24-12-2021 at 08:29
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668988&tid=158187&author=teodor]Monoamine,

I have enough quantity of SOCl2 and th ...
24-12-2021 at 03:48
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669033&tid=158187&author=Bedlasky]Very impressive work Monoamine! I really enjoyed r ...
24-12-2021 at 03:37
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669078&tid=158187&author=Alucard]

It's very strange cause Na2S2O7 melts about 400 ...
23-12-2021 at 13:31
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
Very interesting idea to use chlorosulfonic acid as a catalyst teodor! I don't know if it also works ...
21-12-2021 at 04:53
by: Monoamine
Some afterthoughts
The thionyl chloride was sealed into glass ampules (made from test tubes) for long term storage. The ...
19-12-2021 at 07:32
by: Monoamine
Nitric Acid and Silver Nitrate
or more specifically, when you spill silver nitrate on your hand
then expose it to sunlight before ...
19-12-2021 at 00:51
by: Monoamine
Breaking a stable emulsion
This does not sound like an emulsion to me...
If your solution becomes turbit when adding more wate ...
18-12-2021 at 08:49
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
Hi teodor. Do you know how much air (do you mean O[sub]2[/sub]?) is needed for this to occur? The re ...
18-12-2021 at 00:09
by: Monoamine
Help with FT-IR spectra
There's a peak near 1700 cm-1 this is a very strong hint that your comopound contains a carbonyl (an ...
17-12-2021 at 06:54
by: Monoamine
Discussion
Well, it seems that this method works and is pretty efficient, in the sense that almost no SCl[sub]2 ...
16-12-2021 at 14:52
by: Monoamine
Successful 2 in 1 synthesis: Optimized home-synthesis of SOCl2. Phase II.
To my surprise, the colour in flask B from before had changed from a dark purple/brown to a very pal ...
16-12-2021 at 14:50
by: Monoamine
Successful 2 in 1 synthesis: Optimized home-synthesis of SOCl2. Phase I.
[b]It worked![/b] :D

The previous attempt to make SOCl[sub]2[/sub] didn’t give a pure product, ...
16-12-2021 at 14:43
by: Monoamine
Nitric Acid and Silver Nitrate
Guess what happens when you spill silver nitrate on your hand?

This:
[file]91469[/file]

(A ...
16-12-2021 at 03:13
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668737&tid=158187&author=Lionel Spanner]]
It mostly seems to be used for making chl ...
16-12-2021 at 01:46
by: Monoamine
Thionyl chloride synthesis (SOCl2) from sulfur trioxide (SO3) and sulfur dichloride (SCl2). Phase II.
Next, we stoppered flask B and set it up for distillation to try and fractionally distill off the SC ...
16-12-2021 at 01:38
by: Monoamine
Thionyl chloride synthesis (SOCl2) from sulfur trioxide (SO3) and sulfur dichloride (SCl2). Phase I.
To make SOCl[sub]2[/sub], we followed the synthesis of Georg Brauer on page 382 in “handbook of pr ...
16-12-2021 at 01:30
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
Thank you clearly_not_atara for the tips about reactions of SCl2 with alcohols. Maybe a future proje ...
15-12-2021 at 23:18
by: Monoamine
Discussion: Sulfur dichloride
[file]91445[/file]
SCl[sub]2[/sub] slowly decomposes back into S[sub]2[/sub]Cl[sub]2[/sub] and Cl[ ...
15-12-2021 at 10:18
by: Monoamine
Synthesis of sulfur dichloride (SCl2)
This synthesis is adapted from a youtube video by Extraction&Ire (found [url=https://www.youtube ...
15-12-2021 at 10:12
by: Monoamine
Synthesis of sulfur trioxide (SO3)
This procedure is adapted from the procedure described by user “Garage Chemist”. His original no ...
14-12-2021 at 13:10
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[color=Red]Warning: SO[sub]2[/sub], HCl and Cl[sub]2[/sub] are toxic gasses. SO[sub]3[/sub], SCl[sub ...
14-12-2021 at 12:28
by: Monoamine
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