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A foray into phenethylamines of the Shulgin kind


[Edited on 24-5-2021 by Opylation]
22-5-2021 at 19:51
by: Opylation
Carbon disulfide synthesis (alternative routes)
You can make your own 30% H2O2 using the 3% from the store. It may not be as cheap as getting a jug ...
22-5-2021 at 19:42
by: Opylation
Carbon disulfide synthesis (alternative routes)
Piranha solution should do the trick. Any organic substances that don't get washed away with solvent ...
21-5-2021 at 18:34
by: Opylation
Oxalyl Chloride Challenge
Has someone already mentioned the benzyl alcohol to benzoyl chloride reaction? Then Benzoyl chloride ...
21-5-2021 at 17:47
by: Opylation
A foray into phenethylamines of the Shulgin kind
Beautiful pictures, and great workup. What did you use for your 2,5-dimethoxybenzaldehyde precursor? ...
21-5-2021 at 17:28
by: Opylation
Vilsmeier reagent/POCl3 formation
The indole paper is a pretty good alternative, for indoles. You don't have to work with POCl3 which ...
21-5-2021 at 04:53
by: Opylation
Vilsmeier reagent/POCl3 formation
In interesting alternative to the Vilsmeier–Haack reaction, at least for indoles, involves using i ...
21-5-2021 at 02:10
by: Opylation
Extracting Stevioside from Stevia
If you're trying to keep the plant, some warm water with dish soap sprayed onto the plant daily (mor ...
21-5-2021 at 01:55
by: Opylation
N-acetyl MDA from helional
[Edit]: seems you’re right, not atara. It’s been a while since I read the paper and briefly goin ...
19-5-2021 at 09:32
by: Opylation
Synthesis of Hexahydrocannabinol
[rquote=659568&tid=157403&author=DraconicAcid][rquote=659563&tid=157403&author=stoic ...
19-5-2021 at 00:59
by: Opylation
N-acetyl MDA from helional
Check this paper out. It uses piperonal as the starting material but an intermediary chemical is hel ...
19-5-2021 at 00:41
by: Opylation
Using fungus, fish or fish gills to reduce alcohols amd alkylamines
lol wut? I think the direction you're trying to head in is using enzymes to perform chemical reactio ...
19-5-2021 at 00:33
by: Opylation
Dimethylation of tryptamine via formaldehyde/STAB
I’m probably going to get flack for posting this again, since I just posted it a day or so ago in ...
18-5-2021 at 00:33
by: Opylation
Most toxic compound OTC?
[rquote=659166&tid=155450&author=Fyndium]The major effect of bean toxicity is prominent flat ...
16-5-2021 at 14:24
by: Opylation
Most toxic compound OTC?
Idk if found easily in nature counts for over the counter, but digitoxin found in fox glove (digital ...
16-5-2021 at 14:13
by: Opylation
dialkylation of tryptamine with MeI and CsCO3
Is the issue with over-alkylation just with the beta nitrogen? Or is the issue also with the 1 nitro ...
16-5-2021 at 13:42
by: Opylation
Zinc Thermite?
If your aim is to obtain cheap zinc metal there’s about 5g per penny post 1982

Edit: I’ve see ...
13-12-2020 at 21:05
by: Opylation
Microporous zinc + photo
[rquote=651162&tid=156734&author=vano.kavt]
I have one question. what the number of stars d ...
12-12-2020 at 16:53
by: Opylation
Questions about MPV reduction
I’m not sure about aldehydes but I do have a paper on reduction of esters with magnesium in methan ...
12-12-2020 at 04:25
by: Opylation
Feasibility of creating a nuclear reactor with the aim of transmutation?
I am well aware of the dangers of radiation. I haven’t started anything besides considerations. If ...
12-12-2020 at 04:11
by: Opylation
Feasibility of creating a nuclear reactor with the aim of transmutation?
I was thinking about other ways of producing large amounts of neutrons. Apparently proton accelerato ...
11-12-2020 at 05:37
by: Opylation
How do you draw benzene rings?
[rquote=650924&tid=99305&author=DraconicAcid]I prefer the Greek letter phi to the Ph abbrevi ...
10-12-2020 at 00:00
by: Opylation
More thoughts (rants) on AlCl3 Chlorination of alcohols
[rquote=650891&tid=156704&author=Pumukli]To whom it may concern:

TCT is not equal to TCCA ...
9-12-2020 at 19:09
by: Opylation
More thoughts (rants) on AlCl3 Chlorination of alcohols
There are way easier reagents to use for chlorination of alcohols than aluminum chloride. Have you e ...
9-12-2020 at 00:38
by: Opylation
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
Will if tropinone, or some other analog, is what you’re after I always thought a zn(cu) couple wit ...
7-12-2020 at 18:12
by: Opylation
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