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MAOI(harmine) extraction of tobacco
If I recall correctly, the Pictet-Spengler (probably misspelled) cyclization reaction is quite strai ...
27-9-2013 at 18:17
by: Rich_Insane
Using N-bromosuccinimide to synthesize acyl bromides or carboxamides

[quote]
Volume of what? When you cite, make sure you really do.[/quote]


Oops, my bad, it's f ...
27-9-2013 at 18:13
by: Rich_Insane
Using N-bromosuccinimide to synthesize acyl bromides or carboxamides
I've seen that reference somewhere, but I'm interested in a route that gives direct access to an ami ...
27-9-2013 at 08:40
by: Rich_Insane
Using N-bromosuccinimide to synthesize acyl bromides or carboxamides
I found a reference "Volume 31, Issue 49, 1990, Pages 7237–7240" that describes a radical-mediated ...
27-9-2013 at 08:34
by: Rich_Insane
Protonation of oximes
I'm guessing that this is a really stupid question.
22-9-2013 at 13:51
by: Rich_Insane
How to or where to get alkenes
d-Limonene is pretty common.
21-9-2013 at 17:12
by: Rich_Insane
Protonation of oximes
Hey everyone. I have no formal organic chemistry education, so forgive me if this a very basic quest ...
19-9-2013 at 17:02
by: Rich_Insane
yet another reason to be chemophobic
Er. I am going to sheepishly admit that every so often I take a good whiff of ether. I really like t ...
19-9-2013 at 08:10
by: Rich_Insane
Homemade explosives are for sissies
I've never constructed an actual flamethrower, but in my younger and more foolish days, we would tak ...
19-9-2013 at 07:59
by: Rich_Insane
Seriously, Where To Buy Nitric Acid?
Duda Diesel now sells HNO3, I believe. The costs for ship are so high that it would be infinitely ch ...
19-9-2013 at 07:43
by: Rich_Insane
the basic Strong Acids harm skin?
I've gotten conc. HCl on my skin numerous times. It will not eat away flesh immediately. Run to the ...
10-9-2013 at 16:11
by: Rich_Insane
Please Assist the Noob... Attempting to extract compounds from Plants.
I'd agree that most of these glycosides are hard to extract. Due to the polar nature of the glycosid ...
10-9-2013 at 11:02
by: Rich_Insane
Conversion of Aldehydes to Nitriles
EDIT (Sorry for the double post guys, the site won't let me edit my post)

I'm looking for a littl ...
9-9-2013 at 18:44
by: Rich_Insane
Conversion of Aldehydes to Nitriles
I'm familiar with the 2-Methyl-3-(3,4-methylenedioxyphenyl)propanal route to the amide. In fact, I h ...
8-9-2013 at 18:25
by: Rich_Insane
Conversion of Aldehydes to Nitriles
The aldoxime can be converted (here the oxime will be an intermediate) to the nitrile by dehydration ...
8-9-2013 at 13:18
by: Rich_Insane
Conversion of Aldehydes to Nitriles
I don't plan on working with anything above 500 mmol of substrate, and I plan to not use excess hydr ...
6-9-2013 at 10:31
by: Rich_Insane
Conversion of Aldehydes to Nitriles
Hey everyone,

I came across this article: "A Practical and Cost-Efficient, One-Pot Conversion of ...
5-9-2013 at 18:39
by: Rich_Insane
Hydration of Nitriles to Amides

[quote]
Perhaps you could use it to make a 30% solution of H2O2?
[/quote]

Yes, this is a very ...
2-9-2013 at 20:31
by: Rich_Insane
Hydration of Nitriles to Amides
The compound is sparingly soluble in water at room temperature and soluble in water at 100oC, hence ...
2-9-2013 at 09:35
by: Rich_Insane
Hydration of Nitriles to Amides
Hi guys,

I think there has probably been a thread discussing this particular procedure, because I ...
1-9-2013 at 16:47
by: Rich_Insane
hydrolosis of gaba
What could be hydrolyzed is the diazonium salt of GABA... (Hint hint)
12-8-2013 at 12:50
by: Rich_Insane
3,4-MD-Phenmetrazine
If you are interested in 5HT2A activity, check out "Molecular Pharmacology, December 2006 vol. 70 no ...
6-8-2013 at 21:38
by: Rich_Insane
N,N'-Diisopropylcarbodiimide [Toxicity]
Turns out that DIC is a bit less toxic than DCC (cyclohexyl analogue), because it doesn't appear to ...
6-8-2013 at 21:16
by: Rich_Insane
N,N'-Diisopropylcarbodiimide [Toxicity]
I would if I experienced the symptoms that are labelled (looked through various MSDS files and a tox ...
6-8-2013 at 15:04
by: Rich_Insane
N,N'-Diisopropylcarbodiimide [Toxicity]
Hey guys. I have a question about the toxicity of this compound. I was working with it (doing a TLC ...
6-8-2013 at 14:15
by: Rich_Insane
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