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Help synthesizing icilin
This is pretty serious stuff from a physiological angle.
Milligrams per kilo affect rats, I guess 1 ... |
5-1-2014 at 17:46
by: ScienceSquirrel |
Crystal solvents
They can be labelled in as coordinating ligands;
http://en.wikipedia.org/wiki/Tetrakis%28acetonit ... |
5-1-2014 at 17:34
by: ScienceSquirrel |
Help synthesizing icilin
Looking at the summary on this paper it looks pretty easy if you have access to the starting materia ... |
5-1-2014 at 16:31
by: ScienceSquirrel |
Phenyl isonitrile: the worst stench ever.
Phenyl isocyanide smells awful but it is not really revolting.
MeSeH smells far worse in my opinion ... |
8-12-2013 at 18:04
by: ScienceSquirrel |
The novel and uncharacterized compounds thread.
I have done several crystallisations using the Wikipedia solubility table data and found that they w ... |
8-12-2013 at 17:54
by: ScienceSquirrel |
The true mad science, hydrogen azide distillation
The Victorian period was a great time for amateur science.
Great discoveries were made by amateurs ... |
6-12-2013 at 15:03
by: ScienceSquirrel |
Nelson Mandela
I am not sure if this is the best place to put this but Nelson Mandela achieved a lot in his life fo ... |
5-12-2013 at 17:44
by: ScienceSquirrel |
Isolating Paracetamol (Acetaminophen) from medicine
[rquote=309977&tid=27721&author=TheChemiKid]I used 300 mL of hardware store denatured alcoho ... |
5-12-2013 at 13:25
by: ScienceSquirrel |
Amyl Acetate Adduction Help!
Amyl acetate will not form an adduct with potassium metabisulphite or anything else I can think of i ... |
3-12-2013 at 08:17
by: ScienceSquirrel |
reaction between thiocyanate and nitric acid
You could try extracting it into ether, ethyl acetate, toluene, carbon disulphide, etc.
I doubt tha ... |
2-12-2013 at 13:35
by: ScienceSquirrel |
reaction between thiocyanate and nitric acid
It seems that it can generate hydrogen cyanide, hydrogen suphide, etc.
http://incipiat.wordpress.co ... |
2-12-2013 at 13:08
by: ScienceSquirrel |
dimethyl mercury synthesis
Metallic mercury is not very toxic as it is quite unreactive.
It had a lot of uses in the 17th to 1 ... |
26-11-2013 at 13:40
by: ScienceSquirrel |
Purify chloroxylenol from dettol
No
You are going to be left with the pine oil, castor oil soap and caramel mixed in with your chlor ... |
26-11-2013 at 07:42
by: ScienceSquirrel |
Purify chloroxylenol from dettol
This would be fairly easy in a good laboratory.
Add dilute sulphuric acid to the Dettol until it is ... |
26-11-2013 at 06:42
by: ScienceSquirrel |
Easy Sodium alum?
I think the best way to go would be to mix a warm solution of ammonium sulphate with a warm solution ... |
21-11-2013 at 16:53
by: ScienceSquirrel |
HCl + AgNO3 = HNO3 + AgCl : How?
[rquote=307682&tid=27325&author=AJKOER]Those acquainted with hydrometallury are acquainted w ... |
18-11-2013 at 17:36
by: ScienceSquirrel |
Ideal substitute for rocket fuel.
Practical amateur rocket fuels tend to be a solid mixture of a fuel and an oxidiser.
Zinc powder an ... |
18-11-2013 at 14:32
by: ScienceSquirrel |
Truvia Recrystallization (with interesting supersaturation)
Any strong acid is going to mash up stevioside.
It will cleave those glucose units off and then mas ... |
24-10-2013 at 13:50
by: ScienceSquirrel |
Titanium (III) Potassium Alum: failed attempt
It seems that caesium titanium alum is known;
http://scitation.aip.org/content/aip/journal/jcp/10 ... |
23-10-2013 at 08:20
by: ScienceSquirrel |
aspirin synthesis without acetyl anhydride
You are never going to be able to oxidise a methyl group in the presence of an O acetyl group withou ... |
22-10-2013 at 02:49
by: ScienceSquirrel |
Preparation of Ammonium iron (III) sulphate (ferric alum)
Sorry, my mistake. |
18-10-2013 at 07:43
by: ScienceSquirrel |
Preparation of Ammonium iron (III) sulphate (ferric alum)
The account of the reaction is not quoted but my own.
The experiment is written up in my best JACS' ... |
17-10-2013 at 13:41
by: ScienceSquirrel |
An oxygen flame in a reducing environment
I suspect that it would work but not in an atmosphere like Titan's.
Too much nitrogen and not enoug ... |
14-10-2013 at 15:53
by: ScienceSquirrel |
solder trouble
In my experience, European fishing sinkers are mainly lead but I think thay can contain small amount ... |
14-10-2013 at 15:34
by: ScienceSquirrel |
KCI and NaNO3 solubility?
Solubility table;
http://en.wikipedia.org/wiki/Solubility_table |
7-10-2013 at 04:47
by: ScienceSquirrel |
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