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Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Thanks, everyone!

I eventually managed to get the flasks vacuum-tight but even at 76mmHg and heat ...
2-7-2022 at 02:05
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
[rquote=674708&tid=158709&author=clearly_not_atara][quote]such as isopropanol[/quote]
I don ...
1-7-2022 at 02:14
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Hi,

I have recently attempted to prepare Böhme's salt, which is N,N-dimethylaminomethyleneiminiu ...
29-6-2022 at 02:19
by: SplendidAcylation
Drying acyl halides with molecular sieves?
Thanks for the responses.

[rquote=674600&tid=158699&author=UC235]There is no way there wo ...
26-6-2022 at 02:08
by: SplendidAcylation
Drying acyl halides with molecular sieves?
[rquote=674594&tid=158699&author=PirateDocBrown]Sieves do not like acids. If you have some h ...
25-6-2022 at 02:16
by: SplendidAcylation
Drying acyl halides with molecular sieves?
Hi,

Having recently prepared benzoyl chloride by the chlorination of benzaldehyde, I was about to ...
24-6-2022 at 14:20
by: SplendidAcylation
Antimony Sulfide
[rquote=673934&tid=15349&author=clearly_not_atara]I honestly cannot think of a single reacti ...
2-6-2022 at 03:07
by: SplendidAcylation
Replacement for Chloroform?
@DocX I doubt OP would be interested in DCM since it too is a halogenated solvent, although it is a ...
25-5-2022 at 02:33
by: SplendidAcylation
Replacement for Chloroform?
[rquote=673676&tid=158603&author=clearly_not_atara][quote]I can't imagine chlorobenzene bein ...
21-5-2022 at 02:14
by: SplendidAcylation
Replacement for Chloroform?
Any particular reason for avoiding chloroform?
My daily glass of chloroform doesn't seem to have do ...
20-5-2022 at 03:17
by: SplendidAcylation
What to do with styrene?
[rquote=673388&tid=158580&author=Antiswat]iirc you can turn styrene oxide - or just styrene ...
11-5-2022 at 06:36
by: SplendidAcylation
Some practical questions about Grignard reactions
[rquote=673316&tid=158575&author=zed]To my recollection, this type synthesis calls for an ad ...
8-5-2022 at 02:28
by: SplendidAcylation
What to do with styrene?
I too have been interested in the potential fun projects involving styrene.

You could convert it ...
7-5-2022 at 05:23
by: SplendidAcylation
Some practical questions about Grignard reactions
@tsjerk

Thanks! That's interesting indeed, I suppose if it works for an unreactive halide like ch ...
6-5-2022 at 02:30
by: SplendidAcylation
Some practical questions about Grignard reactions
Hi,

I am planning to make propiophenone by adding ethyl Grignard reagent to benzonitrile.

I ha ...
4-5-2022 at 02:29
by: SplendidAcylation
BnCl synthesis - Using anhy. CaCl2 as catalyst?
I have been wondering about this myself lately!

I think it would work, as it works for similar re ...
10-4-2022 at 02:04
by: SplendidAcylation
Calculating pH
I find that ChemGuide is all I ever need when it comes to this sort of thing:
https://chemguide.co. ...
9-4-2022 at 03:26
by: SplendidAcylation
Second attempt
Hi,

Since my original post, I have re-attempted this reaction, with great success!

I shall des ...
9-4-2022 at 02:23
by: SplendidAcylation
Magnesium Powder
[rquote=672350&tid=158496&author=macckone]unitednuclear.com

I personally buy bulk metal o ...
28-3-2022 at 14:16
by: SplendidAcylation
1,3,5-trithiane
Nice work!
I do love a write-up with photographs

Well done for working with hydrogen sulfide wit ...
28-3-2022 at 14:13
by: SplendidAcylation
Benzamide from benzoic acid + urea - Problems!
Hi,

Inspired by Smuv's write-up [url=https://www.sciencemadness.org/whisper/viewthread.php?tid=42 ...
23-3-2022 at 03:29
by: SplendidAcylation
Somewhat Unusual Properties of Ammonium Benzoate
[rquote=672138&tid=158476&author=hodges][rquote=672134&tid=158476&author=SplendidAcy ...
22-3-2022 at 03:10
by: SplendidAcylation
Is trichloroisocyanuric acid actually an acid?
Thanks for the replies!

The pKa of cyanuric acid seems to be about 7 according to this:
[url]htt ...
22-3-2022 at 03:03
by: SplendidAcylation
Conversion of APAAN(α-phenylacetoacetonitrile) into BMK
It's interesting that it's so easy to decarboxylate the intermediate carboxylic acid simply by heati ...
22-3-2022 at 02:50
by: SplendidAcylation
Somewhat Unusual Properties of Ammonium Benzoate
That's interesting!
Is there any particular reason you recrystallized the benzoic acid from acetone ...
20-3-2022 at 06:05
by: SplendidAcylation
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