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Ibuprofen - Methyl ester and hydroxamic acid derivatives Thanks very much for this. We're looking at doing some reactions with ibuprofen as well, but this is ...	1-3-2016 at 17:17 by: chemplayer..
Synthesis of sodium cyanide from urine Very topical - we've just been doing some chemistry that was inspired after a hard night on BBQ chic ...	29-2-2016 at 03:45 by: chemplayer..
Schmidt reaction - advice on solvents Yeah our problem is that glassware/equipment we can import but chemicals are damn near impossible du ...	27-2-2016 at 20:32 by: chemplayer..
H2O2 + KI + HCl = unexpected reaction A few things could be getting in the way of your desired reaction: 1. Iodine dissolves fairly rea ...	26-2-2016 at 23:31 by: chemplayer..
Schmidt reaction - advice on solvents Actually we have a bit of PCl3 and we could in theory use this to convert to the acid chloride, but ...	26-2-2016 at 23:00 by: chemplayer..
Schmidt reaction - advice on solvents Thankyou. Ok we'll do a lot more reading now. Still a bit nervous about using a chlorinated solve ...	26-2-2016 at 06:38 by: chemplayer..
Schmidt reaction - advice on solvents Wow it's very honouring that you think we might be doing something commercial with the answer! But n ...	26-2-2016 at 03:47 by: chemplayer..
Schmidt reaction - advice on solvents We want to try a Schmidt reaction starting with an alkyl carboxylic acid and converting to an interm ...	25-2-2016 at 18:21 by: chemplayer..
What to do with a barrel of bleach Can't find a reference but from practise we know that mixing hypochlorite and manganese sulfate give ...	21-2-2016 at 18:34 by: chemplayer..
List some BAD chemistry YouTube videos Statistically our observation is: 0.5-1% of views translate into subscribers (provided you post r ...	20-2-2016 at 20:50 by: chemplayer..
lab art Beautiful.	20-2-2016 at 20:23 by: chemplayer..
Amino acid synthesis If you can start from a halo-acid then there are various options to convert this to a primary amine ...	20-2-2016 at 06:34 by: chemplayer..
What to do with a barrel of bleach Some ideas which might lend themselves to 'industrial scaling': 1. Hydrazine sulfate from bleach/ ...	20-2-2016 at 04:19 by: chemplayer..
Grignard successes and failures Sorry, it wasn't really meant to be a comparison. The point is that different compounds react very d ...	18-2-2016 at 22:05 by: chemplayer..
Grignard successes and failures Good and important topic. We've done a few Grignard reactions now and learned the hard way. Our m ...	18-2-2016 at 19:06 by: chemplayer..
synthesis of methyl iodide from methanol, HCl and sodium iodide? KI in methanol and HCl. That's also very interesting and worth a try. Does anyone think that plai ...	14-2-2016 at 03:54 by: chemplayer..
synthesis of methyl iodide from methanol, HCl and sodium iodide? That's a fair comment AvBaeyer. The problem with the methyl iodide one is going to be that if it tak ...	13-2-2016 at 23:08 by: chemplayer..
synthesis of methyl iodide from methanol, HCl and sodium iodide? Yes we were surprised the yield was so good (65%). We'd played around with AlCl3 to see if it wou ...	13-2-2016 at 18:37 by: chemplayer..
synthesis of methyl iodide from methanol, HCl and sodium iodide? EtI is a nightmare. It seems to be a lot less stable than MeI and turns yellow in a week and brown i ...	13-2-2016 at 16:42 by: chemplayer..
buying from China Actually I'll make one observation about Chinese manufactured products - if you're looking for a goo ...	13-2-2016 at 16:36 by: chemplayer..
synthesis of methyl iodide from methanol, HCl and sodium iodide? Another option if you have elemental iodine but no red phosphorus is to use aluminium foil instead! ...	12-2-2016 at 23:21 by: chemplayer..
buying from China t-Butanol ordered... n-Butanol turned up. Sodium bromide ordered... sodium bromate turned up. Pota ...	12-2-2016 at 22:56 by: chemplayer..
Whats the most dangerous chemical you've ever synthesized? Cyanogen iodide and then attempting to isolate it by vacuum fractionally distilling a solution of it ...	12-2-2016 at 22:50 by: chemplayer..

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