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Salicylic Acid from Northen Willow Bark
Technical-grade salicylic acid obtained from the Kolbe-Schmitt process is already extremely pure: sa ...
22-10-2018 at 10:21
by: digga
Salicylic Acid from Northen Willow Bark
Please consider sublimation of the crude product. The Wikipedia entry states that salicylic acid su ...
22-10-2018 at 07:57
by: digga
Benzene synthesis
[rquote=536457&tid=325&author=digga]I took the three combined runs of raw orange benzene, wa ...
4-10-2018 at 10:26
by: digga
Amateur Chemistry now vs several decades ago
It is way harder now. My dad actually got me Nitric and Sulfuric acids at the drugstore! Their onl ...
2-10-2018 at 13:24
by: digga
Benzene synthesis
[rquote=536522&tid=325&author=S.C. Wack]Biphenyl...go back 14 years...the lowest heat is bes ...
19-9-2018 at 07:26
by: digga
Benzene synthesis
I took the three combined runs of raw orange benzene, washed them with distilled water and dried the ...
18-9-2018 at 08:52
by: digga
Nitric Acid and Silver Nitrate
A useful link for relating the percentage of Nitric Acid by weight from density and temperature:

...
14-9-2018 at 05:36
by: digga
Benzene synthesis
Did a third run. I have been able to reuse the same 1 quart paint can each time. The NAON/Sodium B ...
5-9-2018 at 10:28
by: digga
Benzene synthesis
Ran another batch. Similar results ~60 ml of orange "Tang". Worked the temperature control more ca ...
31-8-2018 at 12:38
by: digga
Benzene synthesis
I just ran the NAOH decarboxylation of Sodium Benzoate last night. I used a paint can over a Walmar ...
30-8-2018 at 10:03
by: digga
Disappointed with College Chemistry
In my experience, albeit almost 50 years ago - in the USA. There was no AP anything. Gen Chem was ...
29-8-2018 at 06:14
by: digga
A set of challenges for home chemists.
As a long time New Englander, I hate seeing anything wasted, whether it's a thing, a thought or a th ...
1-8-2018 at 16:47
by: digga
A set of challenges for home chemists.
I believe that there a series of challenges available for all chemists. Those who arrive at solutio ...
1-8-2018 at 08:58
by: digga
Latest chemical order?
Sodium Benzoate - food grade. I intend to whip up some Benzene. When I was a youth, I could and di ...
11-6-2018 at 10:12
by: digga

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