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Percise temperature non-toxic double boiler fluid?
I was under the impression that inhaling the vapor of it would cause poisoning.
28-1-2012 at 13:57
by: freedompyro
Nitric esters storage behaviour under basic conditions
Triple recrystallized perfectly white ETN will be storage stable for years at room temperature witho ...
28-1-2012 at 13:54
by: freedompyro
Lead Picrate
No anti-acid. This is a scenario of picrate salts catalyzing the breakdown of nitrated materials ren ...
28-1-2012 at 13:39
by: freedompyro
Lead Picrate
Is Lead Picrate compatible in mixing with ETN, MHN and other nitrates or does it act to catalyze it' ...
28-1-2012 at 02:52
by: freedompyro
Percise temperature non-toxic double boiler fluid?
I want a double boiler liquid that I can get to simmer at about 105C. I have some ethylene glycol th ...
28-1-2012 at 01:44
by: freedompyro
TNP Purification
I'm not sure this is outside the acceptable scope of scimad... But does anyone know if any of the pi ...
28-1-2012 at 00:02
by: freedompyro
TNP Purification
TNP manages to stand up to hot H2SO4 quite well... Is a water wash and storing it under water good e ...
27-1-2012 at 23:50
by: freedompyro
Direct WFNA distillation without vacuum
Also, contrary to what people say about doing distillations slowly for low NOX... I find the cleares ...
27-1-2012 at 12:29
by: freedompyro
RFNA > Is it good for anything?
I have technical grade urea.

[rquote=234604&tid=18655&author=Ral123]By mixing EG with RFN ...
27-1-2012 at 12:03
by: freedompyro
Distillation of H2SO4 > What tubing stands up to it?
What contaminants in general cause the yellow coloration? I guess distillation is the only way to ge ...
27-1-2012 at 02:00
by: freedompyro
Direct WFNA distillation without vacuum
Just a theory of mine that I have been wanting to test for a long time. Anyone got any thoughts on t ...
27-1-2012 at 01:11
by: freedompyro
RFNA > Is it good for anything?
RFNA has proved to be nothing but a pain in the neck. Half of the common nitrations will NOX at temp ...
27-1-2012 at 00:32
by: freedompyro
Distillation of H2SO4 > What tubing stands up to it?
Pure 98% H2SO4 should be a slight yellow color according to Wikipedia. Btw, should I have left it sl ...
27-1-2012 at 00:02
by: freedompyro
Distillation of H2SO4 > What tubing stands up to it?
Meh... I'm just being obsessive-compulsive in wanting perfect reagents with no trace contaminants... ...
26-1-2012 at 23:58
by: freedompyro
Distillation of H2SO4 > What tubing stands up to it?
Is there any other types of tubing except glass that can withstand high concentration H2SO4? Aluminu ...
26-1-2012 at 19:14
by: freedompyro
HMTD Decomposition Rate and Recrystallization
LoL... Hilarious... I know Adas from elsewhere.
13-1-2012 at 17:13
by: freedompyro
Lead Picrate
How stable is the anhydrous version of lead picreate? No spontaneous decomposition or anything like ...
13-1-2012 at 02:32
by: freedompyro
HMTD Decomposition Rate and Recrystallization
I have been searching around and I cannot find this information anywhere. Since it was once consider ...
13-1-2012 at 01:44
by: freedompyro
Recovery of K2SO4 from K2SO4/H2SO4/HNO3
Very nice work. Thanks a ton Aqua Fortis!
11-1-2012 at 02:32
by: freedompyro
Failed to stop HNO3 from fuming.
The amount of water vapor the air can hold at a specific temperature != humidity. Humidity is the am ...
8-1-2012 at 13:35
by: freedompyro
Separation of Rebiana and Erythritol
You can get Erythritol from amazon or anywhere. Use google shopping and find 10+ places to buy it.
...
8-1-2012 at 04:08
by: freedompyro
Failed to stop HNO3 from fuming.
Yea, it's very humid here.
Crap... Now I have trace amounts of urea nitrate in my nitric acid. Oh w ...
8-1-2012 at 03:25
by: freedompyro
Separation of Rebiana and Erythritol
Just curious if anyone here has ever attempted to separate Truvia into it's component ingredients. N ...
8-1-2012 at 00:33
by: freedompyro
Failed to stop HNO3 from fuming.
I have been quite annoyed at my HNO3 lately. It likes to red fume during a nitration at as low as 11 ...
7-1-2012 at 23:13
by: freedompyro
Recovery of K2SO4 from K2SO4/H2SO4/HNO3
All that information on boiling points was taken off the potassium sulfate wikipedia page.

With t ...
2-1-2012 at 23:35
by: freedompyro
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