| Search |
| [Next Page] |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I find out When reaction time between 1,1dichloroacetone and benzene in FC increase then yield of (P ... |
13-5-2009 at 01:45
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
[rquote=152782&tid=12162&author=turd]
AmiDe guys, not amiNe.
hector: If you really made ... |
12-5-2009 at 10:48
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I buy (R)-(+)-mandelic acid for both reaction (MeLi reaction and Mandelamide reaction)
For purifica ... |
12-5-2009 at 07:03
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Turd,
Maybe reaction between MeLi and mandelic acid has better Yield but you should accept the pri ... |
12-5-2009 at 00:33
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
[rquote=152603&tid=12162&author=turd]
I don't want to start a discussion on principles, but ... |
10-5-2009 at 14:29
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I want to try mandelamide method but i have question
For making mandelamide we should use (R)-(-)-M ... |
10-5-2009 at 09:06
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
[rquote=152565&tid=12162&author=turd]
Yes, that would be crazy, and that's why my first gue ... |
9-5-2009 at 12:40
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I now mandelamide make L-pac and this is very interesting also has easy route to produce L-pac But y ... |
9-5-2009 at 07:40
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I did Reaction between 1,1 dichloroacetone and benzene in FC and then hydrolyze it and got DL-PAC
b ... |
9-5-2009 at 06:25
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
[rquote=152303&tid=12162&author=Nicodem]I seriously do not know if this thread is supposed t ... |
5-5-2009 at 00:50
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Thanks Sauron(khorb koon)
I know i can build tetrabutyltin but now i should use lab grade tetrabuty ... |
4-5-2009 at 07:49
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
No. FC reaction for make Ph-(Co)-(Co)-Cl has good yield but reaction between MeSnnBu3 and Ph-(Co)-( ... |
4-5-2009 at 05:52
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I did PhCOCOMe reaction many time(because Yield is low) and maybe tonight do final reaction.
After ... |
4-5-2009 at 02:41
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I did acylation again.
I used 170 cc Oxalyl chloride(2 mole) and 89cc Benzene(1 mol) and 50cc CS2 a ... |
3-5-2009 at 10:59
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
[rquote=152198&tid=12162&author=Sauron]Hector, I told you to use CS2 zolvent,
That Rhodiu ... |
3-5-2009 at 07:41
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I didnt use solvent.
I used 85 cc Oxalyl chloride(1 mole) and 89cc Benzene(1 mol)
I did reaction l ... |
3-5-2009 at 07:11
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Yes.all of my chemical is lab grade and without water(all of them are old merck product)
I did agai ... |
3-5-2009 at 04:51
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I used dry glassware and dry AlCl3.
I think some Memgcl decompose in air(i used electronic Pipet bu ... |
3-5-2009 at 01:05
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Thanks Sauron,
I download this books and i am reading that.
also i buy Methylmagnesiumchloride(20% ... |
2-5-2009 at 09:00
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Thanks Sauron.
I dont access to refrence part because admin dont allow to me(yet)
You say right.is ... |
2-5-2009 at 01:23
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I fount Tributyltin chloride(CAS#1461-22-9)here(20$ for 100ml)
Just i should react it with MeMgCl.
... |
1-5-2009 at 07:32
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Really interesting method
But i should prepare nBuMgCl(because i didnt find it here)
I think nBuM ... |
1-5-2009 at 00:10
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
[rquote=152061&tid=12162&author=Sauron]
Any experience with organometallic synthesis, hecto ... |
30-4-2009 at 14:48
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Thanks everybody that guide me in this Topic(Special thanks of Mr.Sauron and panziandi)
Soon i will ... |
30-4-2009 at 12:51
by: hector2000 |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Thanks Mr Sauron,
After react Ph-C(O)-CH(Cl)-CH3 with sodium carbonate i will have Ph-C(O)-C(O)-Me ... |
30-4-2009 at 01:26
by: hector2000 |
| [Next Page] |
