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Improving yields of TMP methylation?
MP of the 6.92 g "much, much purer" crystals was taken, something like 65-67 C. The impure crystals ...		 7-4-2019 at 08:04
by: horribilis
Improving yields of TMP methylation?
Same reaction was attempted under slightly different conditions.

The reflux condenser was topped ...		 6-4-2019 at 17:47
by: horribilis
Improving yields of TMP methylation?
[rquote=607295&tid=147245&author=bipolar][rquote=607294&tid=147245&author=horribilis ...		 3-4-2019 at 03:55
by: horribilis
Improving yields of TMP methylation?
[rquote=607290&tid=147245&author=bipolar]1. IMO, inert atmosphere is unnecessary here.

2. ...		 3-4-2019 at 03:21
by: horribilis
Improving yields of TMP methylation?
Not too long ago I attempted o-methylation with trimethyl phosphate (TMP.) US patent US4453017A was ...		 1-4-2019 at 16:05
by: horribilis

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