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Yield of KClO₃ from boiled bleach
Hi Keras, I did this a couple of months back and from 1270g (circa 1.03 L) of 14-15% sodium hypochlo ... |
19-6-2023 at 10:16
by: Boffis |
Glycine anhydride, its preparation and cleavage to a dipeptide
Hi dettoo456, I'm sorry its taken me a while to get back to you, I've been on holiday without my lap ... |
1-6-2023 at 02:16
by: Boffis |
Michler's Ketone
I have just spotted an interesting compound in relation to the preparation of Michler' ketone, the d ... |
11-5-2023 at 09:21
by: Boffis |
Help identifying these metal ions
First of all what do you mean by "coal waste"? Some younger low rank coals have accumulated much van ... |
5-5-2023 at 03:36
by: Boffis |
Ascorbic acid smell when boiled with chlorate
Chloric acid is a weak acid and the free acid an oxidizing agent; ascorbic acid is a reducing agent. ... |
3-5-2023 at 12:40
by: Boffis |
Preparation of Ketones by Calcium salt Pyrolysis
@ Organikum, is this from personal experience or do you have a reference to the magnetite procedure? ... |
3-5-2023 at 11:31
by: Boffis |
Preparation of Ketones by Calcium salt Pyrolysis
I have just finished a couple of runs with calcium butanoate and got a little pleasant minty smellin ... |
2-5-2023 at 13:25
by: Boffis |
Preparation of Ketones by Calcium salt Pyrolysis
Hi Guys, thankyou for the comments. I have been busy making calcium salts of butanoic acid etc (very ... |
1-5-2023 at 07:45
by: Boffis |
Preparation of Ketones by Calcium salt Pyrolysis
Thanks for the comments guys! I am working on a prepublication write-up at the moment and a second b ... |
19-4-2023 at 11:57
by: Boffis |
Preparation of Ketones by Calcium salt Pyrolysis
3-Pentanone by the pyrolysis of Calcium Propanoate
18th April 2023 Boffis
Over the years the pre ... |
18-4-2023 at 14:17
by: Boffis |
Ethyl Pyruvate from Calcium Pyruvate
Hi tyro; what a really interesting write-up. I have been working with calcium pyruvate recently and ... |
18-4-2023 at 08:31
by: Boffis |
Selective Reduction of a cyclic di-imine species
Hmmm. I thought diazepines were 7 member rings, if you condense benzil with and 1,2-phenylenediamine ... |
11-4-2023 at 12:19
by: Boffis |
Large scale plastic waste PBT plastic hydrolysis experiment
@ Hexabromobenzene; these were interesting experiments! I have carried out a fair amount of work on ... |
23-2-2023 at 02:18
by: Boffis |
Mysterious DEET insect-repellent formulation
Hi SplendidAcylation; Were you using a flat bottom flask (conical or otherwise) on a flat hotplate? ... |
22-2-2023 at 13:59
by: Boffis |
Calcium pyruvate to sodium pyruvate or pyruvic acid
As pointed out above by several posters calcium pyruvate is now a fairly readily available food supp ... |
15-2-2023 at 14:22
by: Boffis |
Replacement for acetonitrile in oxone oxidation
Does anyone have any idea if this method would work on conjugate dienes like sorbic acid and piperin ... |
22-1-2023 at 02:41
by: Boffis |
Synthesis of malonic acid
Hi kmno4. I haven’t replied to this thread earlier as when at home over the Christmas period I was ... |
19-1-2023 at 13:05
by: Boffis |
Can DCM act as a Lewis Acid?
If you have washed the reaction mixture with water then the AlCl3 will have hydrolysed and perform n ... |
20-12-2022 at 01:15
by: Boffis |
DNP synthesis
Firstly EvlRenne; from where did this procedure come? Phenol nitrates easily to the mononitro compou ... |
20-12-2022 at 01:08
by: Boffis |
Nitroguanidine reduction product
Is the stuff floating in the red liquor actually red or just the solution? I checked out Richter vol ... |
16-12-2022 at 09:53
by: Boffis |
Nitroguanidine reduction product
Under rather specific conditions with conventional reducing agents it is possible to reduce some nit ... |
16-12-2022 at 05:50
by: Boffis |
Analogs of haloform reaction?
@Falvin, if you want to get useful responses to a post you need to put a bit more effort into your p ... |
14-12-2022 at 05:11
by: Boffis |
Caffeine: reducing the keto-groups to alkanes
If you check out libgen there are a series of books on heterocyclic compounds and there are at least ... |
14-12-2022 at 00:30
by: Boffis |
Preparation of chlorosulfonic acid derived protecting groups
I have a real hard-copy book on naphthalene chemistry. Throughout the book it describes the preparat ... |
3-12-2022 at 13:45
by: Boffis |
Hydrazine Hydrate turning yellow
You need to be more specific with you details! How does IPA (= isopropyl alcohol I presume) free bas ... |
3-12-2022 at 04:03
by: Boffis |
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