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Ethylamine Synthesis
I haven't read the whole thread so I apologise if I am repeating what others have said, but has the ...
7-5-2023 at 13:16
by: SplendidAcylation
Preparation of dimethylamine
@opylation, I wish that these amine salt weedkillers were available here where I live, it would have ...
6-5-2023 at 13:15
by: SplendidAcylation
Preparation of Ketones by Calcium salt Pyrolysis
[rquote=683683&tid=159494&author=Organikum][rquote=683644&tid=159494&author=Splendid ...
4-5-2023 at 01:34
by: SplendidAcylation
Preparation of Ketones by Calcium salt Pyrolysis
[rquote=683650&tid=159494&author=Boffis]Hi Guys, thankyou for the comments. I have been busy ...
2-5-2023 at 01:43
by: SplendidAcylation
Preparation of Ketones by Calcium salt Pyrolysis
[rquote=683438&tid=159494&author=Fery]Boffis as well SplendidAcylation well done both experi ...
1-5-2023 at 03:59
by: SplendidAcylation
Are you guys using ChatGPT
[rquote=683519&tid=159514&author=violet sin]Personally, I'm steering clear of the AI wave.[/ ...
27-4-2023 at 03:09
by: SplendidAcylation
TheVespiary downed?
Here we are again, folks!
26-4-2023 at 12:47
by: SplendidAcylation
Preparation of Ketones by Calcium salt Pyrolysis
[rquote=683362&tid=159494&author=Boffis]

@SplendidAcylation. Did your iron filings + benz ...
24-4-2023 at 01:28
by: SplendidAcylation
Lab clearance for sale on eBay (UK)
Just saw this on eBay, wondered if this is a member; Anyway, if anyone is in the Manchester area the ...
21-4-2023 at 13:22
by: SplendidAcylation
DEET hydrolysis with HCl to diethylamine and toluic acid
Thanks for the info, this is really interesting; I recently did this reaction using sodium hydroxide ...
19-4-2023 at 02:45
by: SplendidAcylation
Preparation of Ketones by Calcium salt Pyrolysis
What a coincidence! While refluxing some iron powder with benzoic acid and acetic acid in a test-tub ...
19-4-2023 at 02:43
by: SplendidAcylation
Simple Reactions with Fluorobenzoic Acid
[rquote=683249&tid=159482&author=clearly_not_atara]Benzene is quite carcinogenic; chlorobenz ...
16-4-2023 at 13:22
by: SplendidAcylation
Simple Reactions with Fluorobenzoic Acid
I think fluorobenzene is a lot safer than benzene! :)

You could turn it into the amide, using ure ...
12-4-2023 at 13:21
by: SplendidAcylation
Hydration of styrene
[rquote=673837&tid=158580&author=Texium][rquote=673835&tid=158580&author=Keras][rquo ...
6-4-2023 at 01:34
by: SplendidAcylation
Preparation of isobutyrophenone by the addition of isopropyl Grignard reagent to benzonitrile (Photo-assay)
[rquote=682868&tid=159451&author=Texium]I wouldn’t recommend plastic syringes with rubber ...
6-4-2023 at 01:25
by: SplendidAcylation
Warfarin syntheses
[rquote=682875&tid=159453&author=DocX][b]Background[/b]
But the internal bleedings caused ...
2-4-2023 at 13:17
by: SplendidAcylation
PDF version
Thanks Tex!

That's a good idea; Do you suppose plastic syringes will be able to handle ether?
I ...
2-4-2023 at 06:12
by: SplendidAcylation
Preparation of isobutyrophenone by the addition of isopropyl Grignard reagent to benzonitrile (Photo-assay)
Hi,

As promised, I have finally completed my write-up for this reaction!
The write-up below is c ...
31-3-2023 at 04:05
by: SplendidAcylation
Calcium cyanurate ---> Cyanamide
[rquote=682819&tid=8594&author=clearly_not_atara]Sulfur would have to come from hydrogen sul ...
30-3-2023 at 13:12
by: SplendidAcylation
Calcium cyanurate ---> Cyanamide
[rquote=682802&tid=8594&author=clearly_not_atara]This would also lead to guanidine and possi ...
29-3-2023 at 12:46
by: SplendidAcylation
Write-up
Hi,

I have repeated the procedures detailed here, and I have had some success in the preparation ...
29-3-2023 at 01:32
by: SplendidAcylation
For those in the UK: kiss goodbye to N2O
I can already see the Daily Mail headlines:

"Air To Be Banned Amid Nitrous Oxide Synthesis Fears" ...
28-3-2023 at 13:09
by: SplendidAcylation
Aluminium and NaOH: what's the gray stuff?
There is another thread on this topic here:
[url]http://www.sciencemadness.org/talk/viewthread.php? ...
22-3-2023 at 03:38
by: SplendidAcylation
DCM vs. Chloroform for Extractions
DCM is approximately twice as soluble as chloroform in water, at room temperature, so you lose a bit ...
4-3-2023 at 14:16
by: SplendidAcylation
Diethylamine and m-Toluic acid from DEET
Excellent write-up!

As elucidated in my recent [url=https://www.sciencemadness.org/whisper/viewth ...
27-2-2023 at 03:37
by: SplendidAcylation
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