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Semicarbazide and Nitrites
Axt:

When you say "130% excess" do you mean 1.3 or 2.3 molar equivalents? (urea being 1 of course ...
27-7-2007 at 05:10
by: agent_entropy
Semicarbazide and Nitrites
Thanks, Axt. Actually that does sound much easier; I suppose the procedure for that method is just ...
26-7-2007 at 12:15
by: agent_entropy
Formula of Ammonium Molybdate
the formula for the hydrate is: (NH4)6Mo7O24 * 4H2O
F.W. 1235.86

(Taken directly from the labe ...
26-7-2007 at 12:06
by: agent_entropy
Semicarbazide and Nitrites
Can anyone direct me to an actual procedure for synthesizing semicarbazide (preferably the hydrochlo ...
26-7-2007 at 07:26
by: agent_entropy
AgNO3......?
@ guy: But I didn't use any ammonia.

My procedure is detailed below:

5 grams of AgNO3 were di ...
10-10-2006 at 16:31
by: agent_entropy
AgNO3......?
Sorry, I typed the reaction in wrong, forgot the coefficients, but I did do the calculations with th ...
10-10-2006 at 04:56
by: agent_entropy
AgNO3......?
I tried the NaOH and sugar method for silver recovery, the one that garage chemist suggested, but I ...
9-10-2006 at 17:58
by: agent_entropy
Caro's Acid-an archive
[quote][i]Originally posted by Fleaker[/i]
I should like to note, peroxysulfuric acid is a great an ...
24-9-2006 at 20:42
by: agent_entropy
h202 concentration?
So what sort of filter SHOULD be used for filtering the ice out of H2O2 when concentrating by the fr ...
23-9-2006 at 15:31
by: agent_entropy
AC and DC Electrolysis
Thanks everyone. Very helpful. I didn't realize that nitrogen oxides could also be yellow in solut ...
19-9-2006 at 09:53
by: agent_entropy
AC and DC Electrolysis
I am trying to speed up reaction time for dissolving silver in nitric acid to make silver nitrate, s ...
18-9-2006 at 22:01
by: agent_entropy
HMTD synth... Second Product?
It just finally ocurred to me that citric acid is not very soluble in methanol, and now I see that c ...
6-9-2006 at 12:16
by: agent_entropy
HMTD synth... Second Product?
HMTD was prepared according to COPAE from the sciencemadness library. After the step where the filt ...
4-9-2006 at 19:04
by: agent_entropy
AgNO3......?
Well, I tried the above method with a small chunk of silver metal (~0.65g) and it didn't seem to wor ...
29-8-2006 at 17:13
by: agent_entropy
AgNO3......?
I was trying to think of ways to produce silver nitrate while conserving nitric acid, and this is th ...
29-8-2006 at 08:45
by: agent_entropy
TCCA, Na-DCCA and cyanuric acid
[quote][i]Originally posted by woelen[/i]
This indeed is a very nice experiment. With TCCA, however ...
28-8-2006 at 13:20
by: agent_entropy
Silver acetylide/nitrate
What is still not clear to me is the actual structure of silver acetylide and the double salt. Can ...
20-8-2006 at 21:48
by: agent_entropy
Mechanism of Peroxide Formation?
Does anyone know the general mechanism for the formation of organic peroxides? (or where I can find ...
20-8-2006 at 21:39
by: agent_entropy
Strike anywhere matches from safety matches
You might try using perchlorate instead of chlorate, it will probably be a lot safer as perchlorates ...
20-8-2006 at 20:06
by: agent_entropy
methyl nitrate
So, a "detonation shock" is not a mechanical shock?
11-8-2006 at 05:41
by: agent_entropy
Sensitivity?
The article "The Chemistry of Powders and Explosives" (by Tenney L. Davis, 1943), from the Sciencema ...
10-8-2006 at 05:51
by: agent_entropy
Complexing methanol
About, using CaCl2 and the like to remove water/methanol from a mixture... In what form must it be u ...
2-8-2006 at 10:31
by: agent_entropy
ONTA
I'd love to hear more details on the synthesis, etc. of NTO whenever you get a chance.
31-7-2006 at 12:02
by: agent_entropy
dimanganese heptaoxide based explosives
So, hydrolyzing Mn2O7 in water would produce permanganic acid (right?). My searches for permanganic ...
31-7-2006 at 06:53
by: agent_entropy
dimanganese heptaoxide based explosives
Awesome, rogue chemist, I was wondering how critical the chromosulfuric acid cleaning was.

Did th ...
30-7-2006 at 12:40
by: agent_entropy
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