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allyl alcohol Has anyone thought about trying this reaction with higher poly-hydroxyalkanes and sugar alcohols suc ... |
30-11-2022 at 03:32 by: Boffis |
Bromination of 1,3 benzodioxole to 5-Bromo-1,3-benzodioxole? Hi Pumikli, I think the difference in the numbering is due to the fact it is regarded as a benzo-het ... |
29-11-2022 at 06:30 by: Boffis |
haloform reaction - cinnamic acid from benzylideneacetone Hi Fery et al. While I haven't tried this reaction on benzalacetone type substrates I have recently ... |
27-11-2022 at 12:10 by: Boffis |
1,2,3,4-tetrahydrocarbazole [rquote=678466&tid=159074&author=Fery]Hi Boffis, the experiment was for the beauty of chemis ... |
21-11-2022 at 11:57 by: Boffis |
2,2'-Bipyridine synthesis Hi Diachrymnic, nice write up once again and I like your make-shift retort from copper pipe and fitt ... |
21-11-2022 at 11:48 by: Boffis |
Pyrazine Synthesis? Diachrynic; nice write-up; its a pity about the yield. I may have a go at this synthesis myself when ... |
21-11-2022 at 11:02 by: Boffis |
Formic Acid Dehydration Hi Chemist1357; I had this problem once and did some research into upgrading my formic acid and I fo ... |
21-11-2022 at 09:50 by: Boffis |
Interesting route to 4-methoxyphenol @ tyro; nice work and an excellent write-up. There are echoes of this method in benignium's write-up ... |
13-11-2022 at 13:39 by: Boffis |
1,2,3,4-tetrahydrocarbazole @ Fery; nice write-up once again. Any particular reason why you chose tetrahydrocarbazole as your ta ... |
13-11-2022 at 13:38 by: Boffis |
Synthesis of malonic acid I agree with you kmno4 about the mp of the diacetic acid and I find this route rather implausible to ... |
12-11-2022 at 07:46 by: Boffis |
Synthesis of malonic acid Hi kmno4, thankyou for the paper, I haven't seen this one before but I have looked at, and indeed tr ... |
11-11-2022 at 12:15 by: Boffis |
Removing graphite from glass frit filter Have you tried reversing the flow of water through the frit. If this and Piranha solution don't move ... |
11-11-2022 at 09:36 by: Boffis |
Synthesis of malonic acid Well, carried out a Mp test on my white crystals and got a figure of 93-93.5 C; the compound melted ... |
9-11-2022 at 11:18 by: Boffis |
Phosphorus pentachloride from phosphides Where can you get cyanuric chloride? |
8-11-2022 at 14:58 by: Boffis |
Synthesis of malonic acid @ kmno4; Well I have something to report but I am not quite sure what!!
I ran a 20g batch of beta ... |
8-11-2022 at 14:56 by: Boffis |
Can oxone oxidise MnSO4 to MnO2 ? One further issue to remember when precipitation MnO2 from aqueous solution is that higher Mn oxides ... |
5-11-2022 at 03:05 by: Boffis |
Does triiodoethanol exist? Interestingly and coincidentally today I spotted some information on 1,1,1-tri-iodoethane or as he c ... |
1-11-2022 at 03:35 by: Boffis |
Synthesis of malonic acid Well the proposed nitric acid oxidation of beta alanine with a trace of nitrite to act as catalyst s ... |
31-10-2022 at 12:18 by: Boffis |
Synthesis of malonic acid While I agree that malonic acid is one of those simple organic building blocks that is best bought I ... |
28-10-2022 at 10:58 by: Boffis |
Pyrazine Synthesis? Hi Diachrynic; the Mp issue was rather my point about investigating my material. Curiously the cryst ... |
28-10-2022 at 06:49 by: Boffis |
Synthesis of malonic acid Hi andyloris, give me a few days and I will track down the various references but I seem to recall t ... |
25-10-2022 at 12:07 by: Boffis |
Synthesis of malonic acid Since acrolein preparation is no joke and yields are not great in laboratory scale procedures as muc ... |
25-10-2022 at 10:28 by: Boffis |
Pyrazine Synthesis? A quick up-date; I tried the ether extraction of the remaining oxidized liquor that hopefully contai ... |
24-10-2022 at 12:35 by: Boffis |
Arsenic and TCCA Back to the OP's question. I noticed recently something I had almost forgotten about. The old method ... |
22-10-2022 at 05:13 by: Boffis |
Cesium hexafluorozirconate - Cs2[ZrF6] Etches glass, Yep that sounds more like a fluoro complex. I don't know how soluble the sulphato-comp ... |
15-10-2022 at 00:58 by: Boffis |
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